Chiral Separation of Four Piperidinic Benzoxazolinone Compounds by CE and LC

被引：0

作者：

Emmanuelle Lipka

Claude Vaccher

Jean-Paul Bonte

Catherine Foulon

机构：

[1] Université de LILLE 2,Laboratoire de Chimie Analytique

来源：

Chromatographia | 2009年 / 69卷

关键词：

Capillary electrophoresis; Column liquid chromatography; Polysaccharide CSP; Highly sulfated cyclodextrins; Chiral separation of piperidinic benzoxazolinones;

D O I：

暂无

中图分类号：

学科分类号：

摘要：

Capillary electrophoresis with negatively charged cyclodextrins and high performance liquid chromatography on polysaccharide chiral stationary phases have been explored for the enantioseparation of chiral piperidinic benzoxazolinone compounds. Operational parameters such as the nature and the concentration of the chiral selectors in CE and the nature of the polysaccharide stationary phase and the composition of the mobile phase in LC were varied in order to achieve the separation of the all four concerning compounds. Limits of detection and quantification of both methods were evaluated under the optimal conditions.

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页码：903 / 909

页数：6

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