Facile synthesis of small crystal ZSM-5 zeolite by acid-catalyzed hydrolysis of tetraethylorthosilicate

被引:0
|
作者
YaJing Wu
XiaoQian Ren
YouDong Lu
Jun Wang
机构
[1] Nanjing University of Technology,State Key Laboratory of Materials
来源
Science in China Series B: Chemistry | 2009年 / 52卷
关键词
hydrolysis; hydrothermal crystal growth; small crystal ZSM-5; tetraethylorthosilicate;
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学科分类号
摘要
Small crystal zeolites ZSM-5 with sizes of 150–300 nm were synthesized using the colloidal silicate precursors as the silica source created by the acid-catalyzed hydrolysis of tetraethylorthosilicate with tetrapropylammonium bromide as the structure-directing agent within a short crystallization time of 20–35 h. The precursors and final products were detected by XRD, SEM, ICP and DLS.
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页码:549 / 551
页数:2
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