Status of the crystallography beamlines at PETRA III

被引:0
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作者
Anja Burkhardt
Tim Pakendorf
Bernd Reime
Jan Meyer
Pontus Fischer
Nicolas Stübe
Saravanan Panneerselvam
Olga Lorbeer
Karolina Stachnik
Martin Warmer
Philip Rödig
Dennis Göries
Alke Meents
机构
[1] Photon Science,Deutsches Elektronen
关键词
Beam Size; Grazing Angle; Beam Position Monitor; Macromolecular Crystallography; Automatic Sample Changer;
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摘要
Since 2013, three beamlines for macromolecular crystallography are available to users at the third-generation synchrotron PETRA III in Hamburg: P11, P13 and P14, the latter two operated by EMBL. Beamline P11 is operated by DESY and is equipped with a Pilatus 6M detector. Together with the photon flux of \documentclass[12pt]{minimal} \usepackage{amsmath} \usepackage{wasysym} \usepackage{amsfonts} \usepackage{amssymb} \usepackage{amsbsy} \usepackage{mathrsfs} \usepackage{upgreek} \setlength{\oddsidemargin}{-69pt} \begin{document}$ 2\times 10^{13}$\end{document} ph/s provided by the very brilliant X-ray source of PETRA III, a full data set can be typically collected in less than 2min. P11 provides state-of-the-art microfocusing capabilities with beam sizes down to \documentclass[12pt]{minimal} \usepackage{amsmath} \usepackage{wasysym} \usepackage{amsfonts} \usepackage{amssymb} \usepackage{amsbsy} \usepackage{mathrsfs} \usepackage{upgreek} \setlength{\oddsidemargin}{-69pt} \begin{document}$ 1\times 1$\end{document} μ m2, which makes the beamline ideally suited for investigation of microcrystals and serial crystallography experiments. An automatic sample changer allows fast sample exchange in less than 20s, which enables high-throughput crystallography and fast crystal screening. For sample preparation, an S2 biosafety laboratory is available in close proximity to the beamline.
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