Molecular and crystal structure of 4-trifluoro-2-[2-(4-fluorophenyl)hydrazine-1-ylidene]-1-(thiophen -2-yl)butane-1,3-dione

被引：0

作者：

A. M. Magerramov

R. A. Alieva

V. I. Mardanova

F. M. Chyragov

A. V. Kurbanov

K. A. Potekhin

机构：

[1] Baku State University,

[2] Vladimir State Humanitarian University,undefined

来源：

Journal of Structural Chemistry | 2012年 / 53卷

关键词：

single crystal X-ray diffraction; crystal structure; β-diketone; 4-trifluoro-2-[2-(4-fluorophenyl)hydrazine-1-ylidene]-1-(thiophen-2-yl)butane-1,3-dione;

D O I：

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摘要：

Single crystal X-ray diffraction is used to determine the crystal and molecular structure of 4-trifluoro-2-[2-(4-fluorophenyl)hydrazine-1-ylidene]-1-(thiophen-2-yl)butane-1,3-dione. Crystallographic data for C14H8F4N2O2S are as follows: a = 8.2723(6) Å, b = 9.3009(7) Å, c = 9.9895(7) Å; α = 79.224(2)°, β = 75.851(2)°, γ = 72.337(2)°. Triclinic crystal system, P-1 space group, dx = 1.622 g/cm3, V = 704.83(9) Å3, μ = 0.286 mm−1, crystal size 0.30×0.20×0.20 mm, R1 = 0.0891, wR2 = 0.1989.

引用

页码：202 / 205

页数：3

共 16 条

[1]

Baidina I. A.(2007)undefined J. Struct. Chem. 48 494-499

[2]

Kuratieva N. V.(2005)undefined J. Struct. Chem. 46 154-undefined

[3]

Stabnikov P. A.(2003)undefined J. Struct. Chem. 44 642-undefined

[4]

Gromilov S. A.(2011)undefined Koordinats. Khim. 37 268-undefined

[5]

Shishkina S. V.(2011)undefined Koordinats. Khim. 37 46-undefined

[6]

Baumer V. N.(undefined)undefined undefined undefined undefined-undefined

[7]

Shishkin O. V.(undefined)undefined undefined undefined undefined-undefined

[8]

Sharikova O. G.(undefined)undefined undefined undefined undefined-undefined

[9]

Naumov D. Yu.(undefined)undefined undefined undefined undefined-undefined

[10]

Shvedenkov Yu. G.(undefined)undefined undefined undefined undefined-undefined

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