Synthesis and Characterization of Ferromagnetic Nickel Nanoparticles

被引:0
作者
T. G. Altınçekiç
İ. Boz
A. C. Basaran
B. Aktaş
S. Kazan
机构
[1] Istanbul University Avcılar,Department of Chemical Engineering, Faculty of Engineering
[2] Gebze Institute of Technology,Department of Physics
来源
Journal of Superconductivity and Novel Magnetism | 2012年 / 25卷
关键词
Ni nanoparticles; Ferromagnetic resonance; Polyol process;
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学科分类号
摘要
Nickel nanoparticles on mass production scale have been prepared using a modified polyol process with Ni(CH3COO)2⋅4H2O, NaOH, 1,2 propandiol and hydrazinium hydroxide (N2H4∗H2O). A mixture of face centered cubic (fcc) metallic nickel nanoparticles with 12 nm diameter were obtained. We have experimentally studied the structure of nanoparticle by X-ray and Scanning Electron Microscopy (SEM, EDS). The magnetic properties of the prepared Ni film have been studied by Ferromagnetic Resonance (FMR) technique, Vibrating Sample Magnetometer (VSM) and Vector Network Analyzer (VNA). The effective g-factor and magnetic anisotropy constant were determined as geff=2.25 and Keff=85 Oe, respectively.
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页码:2771 / 2775
页数:4
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