Zirconium(IV) 4-sulphophenylethyliminobismethylphosphonate as an efficient and reusable catalyst for one-pot synthesis of 3,4-dihydropyrimidones under solvent-free conditions

被引：0

作者：

Xin-Bin Yang

Xiang-Kai Fu

Yu Huang

Ren-Quan Zeng

机构：

[1] Southwest University,Department of Chemistry, Rongchang Campus

[2] Southwest University,School of Chemistry and Chemical Engineering

[3] Ningxia Medical University,Pharmacy College

来源：

Chemical Papers | 2011年 / 65卷

关键词：

zirconium; phosphonate; acid catalyst; 3,4-dihydropyrimidones; solvent-free;

D O I：

暂无

中图分类号：

学科分类号：

摘要：

Zirconium(IV) 4-sulphophenylethyliminobismethylphosphonate (ZSBEDP) was prepared and characterised by elemental analysis, IR, TG-DSC, and XRD. ZSBEDP was found to be an efficient catalyst for the Biginelli reaction of aromatic aldehyde, ethyl acetoacetate, and urea or thiourea under solvent-free conditions so as to give 3,4-dihydropyrimidones in good to excellent yields. The catalyst can be separated by simple filtration and reused without significant loss of its catalytic activity.

引用

页码：829 / 834

页数：5

共 50 条

[11] Hydrotalcite: A novel and reusable solid catalyst for one-pot synthesis of 3,4-dihydropyrimidinones and mechanistic study under solvent free conditions
Lal, Jaggi
Sharma, Monika
Gupta, Savita
Parashar, Priyanka
Sahu, Pramod
Agarwal, D. D.
JOURNAL OF MOLECULAR CATALYSIS A-CHEMICAL, 2012, 352 : 31 - 37
[12] A novel polymeric catalyst for the one-pot synthesis of xanthene derivatives under solvent-free conditions
Maleki, Behrooz
Barzegar, Shahram
Sepehr, Zeinalabedin
Kermanian, Mina
Tayebee, Reza
JOURNAL OF THE IRANIAN CHEMICAL SOCIETY, 2012, 9 (05) : 757 - 765
[13] A novel polymeric catalyst for the one-pot synthesis of xanthene derivatives under solvent-free conditions
Behrooz Maleki
Shahram Barzegar
Zeinalabedin Sepehr
Mina Kermanian
Reza Tayebee
Journal of the Iranian Chemical Society, 2012, 9 : 757 - 765
[14] Borax: An Ecofriendly and Efficient Catalyst for One-Pot Synthesis of 3,4-Dihydropyrimidine-2(1H)-ones under Solvent-Free Conditions
Nath, Jayashree
Chaudhuri, Mihir K.
SYNTHETIC COMMUNICATIONS, 2010, 40 (20) : 2976 - 2982
[15] One-pot synthesis of xanthene derivatives under solvent-free conditions
Dabiri, Minoo
Azimi, Seyyedeh C.
Bazgir, Ayoob
CHEMICAL PAPERS, 2008, 62 (05): : 522 - 526
[16] One-pot synthesis of xanthene derivatives under solvent-free conditions
Minoo Dabiri
Seyyedeh C. Azimi
Ayoob Bazgir
Chemical Papers, 2008, 62 : 522 - 526
[17] Nanocrystalline MgAl2O4 as an efficient catalyst for one-pot synthesis of multisubstituted imidazoles under solvent-free conditions
Safari, Javad
Akbari, Zahra
Naseh, Simin
JOURNAL OF SAUDI CHEMICAL SOCIETY, 2016, 20 : S250 - S255
[18] Al(OTf)3 as an Efficient Catalyst for One-Pot Synthesis of Primary Diethyl 1-Aminophosphonates Under Solvent-Free Conditions
Sobhani, Sara
Tashrifi, Zahra
SYNTHETIC COMMUNICATIONS, 2009, 39 (01) : 120 - 131
[19] Bronsted acidic ionic liquid as an efficient and reusable catalyst for one-pot synthesis of 1-amidoalkyl 2-naphthols under solvent-free conditions
Hajipour, Abdol R.
Ghayeb, Yosof
Sheikhan, Nafisehsadat
Ruoho, Arnold E.
TETRAHEDRON LETTERS, 2009, 50 (40) : 5649 - 5651
[20] Ammonium Oxalate as an Efficient Catalyst for One-Pot Synthesis of Tetrahydrobenzo [a]xanthen-11-one Derivatives Under Solvent-Free Conditions
Esfahani, Hamid R. M.
Foroughifar, Naser
Mobinikhaledi, Akbar
Moghanian, Hassan
SYNTHESIS AND REACTIVITY IN INORGANIC METAL-ORGANIC AND NANO-METAL CHEMISTRY, 2013, 43 (06) : 752 - 755

← 1 2 3 4 5 →