Crystal Structure of 2-(Pyridin-4-yl)-5-(Undecylthio)-1,3,4-Oxadiazole

被引：0
|
作者：
Z.-H. Shen
Q. Wang
Z.-H. Sun
H.-K. Wu
C.-X. Tan
J.-Q. Weng
X.-H. Liu
机构：
[1] Zhejiang University of Technology,College of Chemical Engineering
来源：
Journal of Structural Chemistry | 2018年 / 59卷
关键词：
heterocycle; synthesis; crystal structure;
D O I：
暂无
中图分类号：
学科分类号：
摘要：
The title compound 2-(pyridin-4-yl)-5-(undecylthio)-1,3,4-oxadiazole (C18H27ON3S) is synthesized, and its structure is confirmed by 1H NMR, MS, elemental analyses and X-ray diffraction. It crystallizes in the monoclinic system, space group P2(1)/c with a = 24.453(17) Å, b = 10.604(7) Å, c = 7.095(5) Å, β = 91.60(2)°, V = 1839(2) Å3, Z = 4, and R = 0.086 for 2295 observed reflections with I > 2σ(I). The preliminary biological test shows that the title compound has good activity against Pythium ultimum with inhibitory to be 77.78%.
引用
收藏
页码：1236 / 1240
页数：4
相关论文
共 50 条
  • [21] Synthesis and Crystal Structure of 2-(4-Decarboxydehydroabietyl)-5-p-tolyl-[1,3,4]-oxadiazole
    苏桂发
    关一富
    黄婉云
    王恒山
    潘英明
    Chinese Journal of Structural Chemistry, 2009, (07) : 881 - 885
  • [22] Synthesis and Crystal Structure of 2-(4-Decarboxydehydroabietyl)-5-p-tolyl-[1,3,4]-oxadiazole
    Su Gui-Fa
    Guan Yi-Fu
    Huang Wan-Yun
    Wang Heng-Shan
    Pan Ying-Ming
    CHINESE JOURNAL OF STRUCTURAL CHEMISTRY, 2009, 28 (07) : 881 - 885
  • [23] Synthesis and Crystal Structure of 4-Phenyl-3-(pyridin-4-yl)-1H-1,2,4-triazole-5(4H)-thione
    Gao, Wei
    Guo, Feng-Peng
    Yang, Jing
    ASIAN JOURNAL OF CHEMISTRY, 2014, 26 (07) : 2083 - 2085
  • [24] Syntheses and Crystal Structures of Two New Complexes Generated from 2-((Pyridin-3-ylmethyl)thio)-5-(6-quinolinyl)-1,3,4-oxadiazole and Ag~Ⅰ Salts
    吴祥雯
    尹诗
    马建平
    结构化学, 2016, 35 (12) : 1894 - 1901
  • [25] Synthesis, crystal and molecular structure, DFT and antifungal activity studies of (E)-2-(3-methoxy-4-((6-(trifluoromethyl)pyrimidin-4-yl)oxy) styryl)-5-((2-(trifluoromethyl)benzyl)thio)-1,3,4-oxadiazole
    Wu, Wenneng
    An, Jiansong
    Pan, Nianjuan
    Liu, Chunyi
    Chen, Haijiang
    Fei, Qiang
    Gan, Xiuhai
    Zhou, Zhixu
    JOURNAL OF MOLECULAR STRUCTURE, 2024, 1316
  • [26] Syntheses and Crystal Structures of Two New Complexes Generated from 2-((Pyridin-3-ylmethyl)thio)-5-(6quinolinyl)-1,3,4-oxadiazole and AgI Salts
    Wu Xiang-Wen
    Yin Shi
    Ma Jian-Ping
    CHINESE JOURNAL OF STRUCTURAL CHEMISTRY, 2016, 35 (12) : 1894 - 1901
  • [27] 2-(allylthio)-5-(5-phenyl-1H-pyrazol-3-yl)-1,3,4-oxadiazole: Synthesis, single crystal XRD, spectroscopic characterization, antidiabetic activity, DFT and ADMET studies
    El Hassani, Issam Ameziane
    Brandan, Silvia A.
    Mortada, Salma
    Arshad, Suhana
    Romano, E.
    Ramli, Youssef
    Mague, Joel T.
    Faouzi, My El Abbes
    Karrouchi, Khalid
    Ansar, M'hammed
    JOURNAL OF MOLECULAR STRUCTURE, 2024, 1295
  • [28] Crystal structure of 9-butyl-6-[2-(pyridin-4-yl)ethenyl]carbazol-3-amine
    Zhang, Ping
    Bai, Xiang-Yang
    Zhang, Ting
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2015, 71 : O345 - U579
  • [29] Crystal structure of 3-[(4-benzylpiperazin-1-yl)methyl]-5-(thiophen-2-yl)-2,3-dihydro-1,3,4-oxadiazole-2-thione
    Al-Omary, Fatmah A. M.
    El-Emam, Ali A.
    Ghabbour, Hazem A.
    Kumar, C. S. Chidan
    Quah, Ching Kheng
    Fun, Hoong-Kun
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2015, 71 : O175 - +
  • [30] Synthesis,Crystal Structure and Fluorescent Properties of a Cadmium(Ⅱ) Complex with 3-(Pyridin-4-yl)-5-(pyrazin-2-yl)-1H-1,2,4-triazole
    王玉芳
    孙小媛
    耿俊磊
    结构化学, 2016, 35 (03) : 397 - 403
12345