Crystal Structure of 2-(Pyridin-4-yl)-5-(Undecylthio)-1,3,4-Oxadiazole

被引：0
|
作者：
Z.-H. Shen
Q. Wang
Z.-H. Sun
H.-K. Wu
C.-X. Tan
J.-Q. Weng
X.-H. Liu
机构：
[1] Zhejiang University of Technology,College of Chemical Engineering
来源：
Journal of Structural Chemistry | 2018年 / 59卷
关键词：
heterocycle; synthesis; crystal structure;
D O I：
暂无
中图分类号：
学科分类号：
摘要：
The title compound 2-(pyridin-4-yl)-5-(undecylthio)-1,3,4-oxadiazole (C18H27ON3S) is synthesized, and its structure is confirmed by 1H NMR, MS, elemental analyses and X-ray diffraction. It crystallizes in the monoclinic system, space group P2(1)/c with a = 24.453(17) Å, b = 10.604(7) Å, c = 7.095(5) Å, β = 91.60(2)°, V = 1839(2) Å3, Z = 4, and R = 0.086 for 2295 observed reflections with I > 2σ(I). The preliminary biological test shows that the title compound has good activity against Pythium ultimum with inhibitory to be 77.78%.
引用
收藏
页码：1236 / 1240
页数：4
相关论文
共 50 条
  • [1] Crystal Structure of 2-(Pyridin-4-yl)-5-(Undecylthio)-1,3,4-Oxadiazole
    Shen, Z. -H.
    Wang, Q.
    Sun, Z. -H.
    Wu, H. -K.
    Tan, C. -X.
    Weng, J. -Q.
    Liu, X. -H.
    JOURNAL OF STRUCTURAL CHEMISTRY, 2018, 59 (05) : 1236 - 1240
  • [2] Synthesis,Crystal Structure and Antifungal Activity of 2-((2-Fluorobenzyl)thio)-5-(pyridin-4-yl)-1,3,4-oxadiazole
    孙国香
    石延霞
    翟志文
    孙召慧
    翁建全
    谭成侠
    刘幸海
    李宝聚
    结构化学, 2016, 35 (12) : 1855 - 1859
  • [3] Synthesis, Crystal Structure and Antifungal Activity of 2-((2-Fluorobenzyl)thio)-5-(pyridin-4-yl)-1,3,4-oxadiazole
    Sun Guo-Xiang
    Shi Yan-Xia
    Zhai Zhi-Wen
    Sun Zhao-Hui
    Weng Jian-Quan
    Tan Cheng-Xia
    Liu Xing-Hai
    Li Bao-Ju
    CHINESE JOURNAL OF STRUCTURAL CHEMISTRY, 2016, 35 (12) : 1855 - 1859
  • [4] Crystal structure of 2-(adamantan-1-yl)-5-(4-bromophenyl)-1,3,4-oxadiazole
    Alzoman, Nourah Z.
    El-Emam, Ali A.
    Ghabbour, Hazem A.
    Kumar, C. S. Chidan
    Fun, Hoong-Kun
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2014, 70 : O1231 - +
  • [5] ZnII and CuII complexes generated from 5-(pyridin-4-yl)-3-[2-(pyridin-4-yl)ethyl]-1,3,4-oxadiazole-2(3H)-thione
    Zhao, Hang-Ju
    Ma, Jian-Ping
    Liu, Qi-Kui
    Dong, Yu-Bin
    ACTA CRYSTALLOGRAPHICA SECTION C-STRUCTURAL CHEMISTRY, 2013, 69 : 716 - +
  • [6] Crystal structures and Hirshfeld surface analysis of 2-(adamantan-1-yl)-5-(4-fluoropheny1)-1,3,4-oxadiazole and 2-(adamantan-1-yl)-5-(4-chlorophenyl)-1,3,4-oxadiazole
    Al-Wahaibi, Lamya H.
    Alsfouk, Aisha
    El-Emam, Ali A.
    Blacque, Olivier
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2019, 75 : 611 - +
  • [7] 2-(Adamantan-1-yl)-5-(4-nitrophenyl)-1,3,4-oxadiazole
    El-Emam, Ali A.
    Kadi, Adnan A.
    El-Brollosy, Nasser R.
    Ng, Seik Weng
    Tiekink, Edward R. T.
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2012, 68 : O795 - U2666
  • [8] Crystal structure of 2-{[(naphthalen-1-yl)oxy]methyl}-5-(2,4,5-trifluorophenyl)-1,3,4-oxadiazole
    Govindhan, Muniyappan
    Subramanian, Kathavarayan
    Viswanathan, Vijayan
    Velmurugan, Devadasan
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2015, 71 : O190 - +
  • [9] Tetraaquabis(2-{[5-(pyridin-4-yl)-1,3,4-oxadiazol-2-yl]sulfanyl}acetato)iron(II)
    Wang, Hai-Rong
    Li, Guo-Ting
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2011, 67 : M1457 - U1426
  • [10] 4-[5-(Pyridin-4-yl)-1,3,4-oxadiazol-2-yl]pyridinium benzoate
    Han, Meng Ting
    Zhang, Yuan
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2011, 67 : O447 - U1343
12345