Optimization of microwave-assisted extraction of solanesol from potato leaves and stems

被引:0
作者
Tong Chen
Xuegang Sun
Wen Xiao
Xiaojuan Liu
Wei Zhang
Kai Ma
Yinrong Zhu
机构
[1] Gansu Agricultural University,College of Forestry
[2] Gansu Agricultural University,College of Science
[3] Gansu Agricultural University,College of Life Science and Technology
来源
Medicinal Chemistry Research | 2010年 / 19卷
关键词
Microwave-assisted extraction; Solanesol; Potato leaves and stems; RP-high performance liquid chromatography;
D O I
暂无
中图分类号
学科分类号
摘要
Microwave-assisted extraction (MAE) was developed for the fast extraction of solanesol from potato leaves and stems. The ratio of raw material to ethanol, extraction time, extraction temperature, and microwave irradiation power were interdependent. The yield of solanesol reached its maximum 98.57% with 1:8.0 g/ml, 40 min, 55°C, and 2.0 KW, respectively. MAE was comparable to other extraction methods, including solvent extraction, heat-reflux, and Soxhlet-extraction. MAE reduced extraction time, solvent consumption, and increased yields of solanesol. Solanesol concentration was performed by RP-high performance liquid chromatography. The method was rapid, simple, accurate, and reproducible.
引用
收藏
页码:732 / 742
页数:10
相关论文
共 38 条
[1]  
Akhter MH(1996)Extraction of salinomycin from finished layers ration by microwave solvent extraction followed by liquid chromatography Analyst (Lond) 121 803-806
[2]  
Croteau LG(2007)Rapid determination of total solanesol in tobacco leaf by ultrasound-assisted extraction with RP-HPLC and ESI-TOF/MS J Pharm Biomed 43 879-885
[3]  
Chena JH(1994)On-line sample preparation for the determination of riboflavin and flavin mononucleotides in food stuffs Analyst (Lond) 119 929-935
[4]  
Liu XP(2002)Synthesis of [3–14C] coenzyme Q10 J Labelled Comp Radiopharm 45 823-829
[5]  
Xu XQ(2008)Antioxidant activity of microwave-assisted extract of longan (Dimocarpus Longan Lour.) peel Food Chem 106 1264-1270
[6]  
Lee FSC(1956)Flue-cured I. Tobacco, isolation of solanesol, an unsaturated ethanol J Am Chem Soc 78 4680-4683
[7]  
Wang XR(2002)Extract and quantitation determination of solanesol from discarded tobacco in Yunnan province J Yunnan Univ Nat Sci 24 151-216
[8]  
Greenway GM(1997)Solid-phase microextracion associated with microwave assisted extraction of food products J High Resolut Chromatogr 20 213-167
[9]  
Kometa N(2008)Analysis of ginsenosides in Panax ginseng in high pressure microwave-assisted extraction Food Chem 110 161-257
[10]  
Hamamura K(1996)Extraction as a method for preparation of vegetable samples for the determination of trace metals by atomic absorption spectrometry Anal Chim Acta 330 251-40