(4-Carbamoylphenyl)boronic acid

被引：3

作者：

Apostolova, Margarita D. ^{[2
]}

Nikolova, Rositsa P. ^{[1
]}

Shivachev, Boris L. ^{[1
]}

机构：

[1] Bulgarian Acad Sci, Cent Lab Mineral & Crystallog, BU-1113 Sofia, Bulgaria

[2] Bulgarian Acad Sci, Inst Mol Biol Acad R Tsanev, BU-1113 Sofia, Bulgaria

来源：

ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE | 2010年 / 66卷

关键词：

CROSS-COUPLING REACTIONS;

D O I：

10.1107/S1600536810014789

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

In the title compound, C7H8BNO3, the molecule lies on an inversion center leading to a statistical disorder of the B(OH)(2) and CONH2 groups. In the crystal structure, molecules are linked by N-H center dot center dot center dot O and O-H center dot center dot center dot O hydrogen bonds, forming sheets parallel to the bc plane. The B(OH)(2) and CONH2 groups are twisted out of the mean plane of the benzene ring by 23.9 (5) and 24.6 (6)degrees, respectively.

引用

页码：O1273 / U249

页数：11

共 17 条

[1] Development of the proteasome inhihitor Veleade™ (Bortezomib) [J].

Adams, J ;

Kauffman, M .

CANCER INVESTIGATION, 2004, 22 (02) :304-311

[2] Boron neutron capture therapy of cancer: Current status and future prospects [J].

Barth, RF ;

Coderre, JA ;

Vicente, MGH ;

Blue, TE .

CLINICAL CANCER RESEARCH, 2005, 11 (11) :3987-4002

[3] PATTERNS IN HYDROGEN BONDING - FUNCTIONALITY AND GRAPH SET ANALYSIS IN CRYSTALS [J].

BERNSTEIN, J ;

DAVIS, RE ;

SHIMONI, L ;

CHANG, NL .

ANGEWANDTE CHEMIE-INTERNATIONAL EDITION, 1995, 34 (15) :1555-1573

[4] New software for searching the Cambridge Structural Database and visualizing crystal structures [J].

Bruno, IJ ;

Cole, JC ;

Edgington, PR ;

Kessler, M ;

Macrae, CF ;

McCabe, P ;

Pearson, J ;

Taylor, R .

ACTA CRYSTALLOGRAPHICA SECTION B-STRUCTURAL SCIENCE CRYSTAL ENGINEERING AND MATERIALS, 2002, 58 :389-397

[5] CRYSTAL-STRUCTURE OF TEREPHTHALAMIDE [J].

COBBLEDICK, RE ;

SMALL, RWH .

ACTA CRYSTALLOGRAPHICA SECTION B-STRUCTURAL CRYSTALLOGRAPHY AND CRYSTAL CHEMISTRY, 1972, B 28 (OCT15) :2893-+

[6] SUPRAMOLECULAR SYNTHONS IN CRYSTAL ENGINEERING - A NEW ORGANIC-SYNTHESIS [J].

DESIRAJU, GR .

ANGEWANDTE CHEMIE-INTERNATIONAL EDITION IN ENGLISH, 1995, 34 (21) :2311-2327

[7]

Enraf-Nonius, 1994, CAD 4 EXPRESS

[8]

Farrugia L.J., 1997, J. Appl. Crystallogr., V30, P565, DOI [10.1107/S0021889897003117, DOI 10.1107/S0021889897003117]

[9]

Farrugia L. J., 1999, Journal of Applied Crystallography, V32, P837, DOI [DOI 10.1107/S0021889812029111, 10.1107/S0021889899006020, DOI 10.1107/S0021889899006020]

[10]

Harms K., 1995, XCAD4

← 1 2 →