Phase structure and residual stress in annealed Cu-W films

被引:0
作者
Wang Yuan [1 ]
Li Xiaohua
Song Zhongxiao
Xu Kewei
Wei Xiuying
机构
[1] Gen Res Inst NonFerrous Met, Res Ctr Energy Mat & Technol, Beijing 100088, Peoples R China
[2] Beijing Univ Technol, Signal & Informat Proc Lab, Beijing 100022, Peoples R China
[3] Xi An Jiao Tong Univ, State Key Lab Mech Behav Mat, Xian 710049, Peoples R China
关键词
Cu-W thin film; phase transition; residual stress; annealing;
D O I
暂无
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
The phase transition of Copper-tungsten films deposited on Si (100) and Al2O3 substrates took place by means of in situ annealing in vacuum chamber at different temperatures. X-ray diffraction (XRD) and the polarization phase shift technique were employed to characterize the microstructure and residual stress of Cu-W films, respectively. The results indicated that the two successive but distinctive stages of phase transition appeared with the change of annealing temperatures, i.e., W (Cu) solution formation and two-phase crystalline (W and Cu) structure formation. The relationship between phase transition and residual stress was investigated, the tensile stress was caused during phase transition, whereas it was released with crystalline growth.
引用
收藏
页码:435 / 439
页数:5
相关论文
共 26 条
[1]  
BERRY RW, 1972, THIN FILM TECHNOLOGY, P189
[2]   The dissociation of an alloy of copper, iron and nickel Further X-ray work [J].
Daniel, V ;
Lipson, H .
PROCEEDINGS OF THE ROYAL SOCIETY OF LONDON SERIES A-MATHEMATICAL AND PHYSICAL SCIENCES, 1944, 182 (A991) :378-387
[3]   METASTABLE SOLID-SOLUTIONS IN VAPOR-DEPOSITED CU-CR, CU-MO, AND CU-W THIN-FILMS [J].
DIRKS, AG ;
VANDENBROEK, JJ .
JOURNAL OF VACUUM SCIENCE & TECHNOLOGY A-VACUUM SURFACES AND FILMS, 1985, 3 (06) :2618-2622
[4]   Plastic properties of thin films on substrates as measured by submicron indentation hardness and substrate curvature techniques [J].
Doerner, M. F. ;
Gardner, D. S. ;
Nix, W. D. .
JOURNAL OF MATERIALS RESEARCH, 1986, 1 (06) :845-851
[5]   THERMAL-CONDUCTIVITY AND THERMAL-EXPANSION OF GRAPHITE FIBER-REINFORCED COPPER MATRIX COMPOSITES [J].
ELLIS, DL ;
MCDANELS, DL .
METALLURGICAL TRANSACTIONS A-PHYSICAL METALLURGY AND MATERIALS SCIENCE, 1993, 24 (01) :43-52
[6]   MEASUREMENT AND INTERPRETATION OF STRESS IN ALUMINUM-BASED METALLIZATION AS A FUNCTION OF THERMAL HISTORY [J].
FLINN, PA ;
GARDNER, DS ;
NIX, WD .
IEEE TRANSACTIONS ON ELECTRON DEVICES, 1987, 34 (03) :689-699
[7]   Model for stress generated upon contact of neighboring islands on the surface of a substrate [J].
Freund, LB ;
Chason, E .
JOURNAL OF APPLIED PHYSICS, 2001, 89 (09) :4866-4873
[8]  
GERMAN GA, 1993, METALL T A, V24, P35
[9]  
GERMAN RM, 1993, ADV POWDER METALLURG, V6, P189
[10]   CRYSTALLIZATION OF CU50W50 AND CU66W34 AMORPHOUS-ALLOYS [J].
GRZETA, B ;
RADIC, N ;
GRACIN, D ;
DOSLIC, T ;
CAR, T .
JOURNAL OF NON-CRYSTALLINE SOLIDS, 1994, 170 (01) :101-104