Synthesis of CuInS2 nanometric powder by reaction in molten KSCN

被引:9
作者
Benchikhi, Mohamed [1 ,2 ]
El Ouatib, Rachida [1 ]
Guillemet-Fritsch, Sophie [2 ]
Chane-Ching, Jean Yves [2 ]
Demai, Jean Jacques [2 ]
Er-Rakho, Lahcen [1 ]
Durand, Bernard [2 ]
机构
[1] Univ Hassan II Casablanca, Lab Physicochim Mat Inorgan, Casablanca, Morocco
[2] Univ Toulouse, CNRS, Inst Carnot CIRIMAT, F-31062 Toulouse 9, France
关键词
Chalcogenide; Semiconductor; Molten salt; Nanoparticles; CU2ZNSNS4; THIN-FILMS; OPTICAL-PROPERTIES; ELECTRODEPOSITION; NANOPARTICLES; THIOCYANATE; CUGASE2; ROUTE;
D O I
10.1016/j.matlet.2014.08.101
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
CuInS2 was synthesized, with a yield of 70% by reaction in molten KSCN at 400 degrees C of CuCl2 and InCl3 with a ratio KSCN/Cu=15. The homogeneous powder obtained is constituted of nano-sized grains (70-100 nm), with a specific surface area of 6 m(2)/g and a band gap Eg of 1.5 eV. (C) 2014 Elsevier B.V. All rights reserved.
引用
收藏
页码:431 / 434
页数:4
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