Simultaneous determination of three azo dyes in food product by ion mobility spectrometry

被引:29
作者
Jiao, Jiandong [1 ,2 ]
Wang, Jinfeng [1 ]
Li, Mingfeng [3 ]
Li, Junqing [2 ]
Li, Qihong [2 ]
Quan, Qinbo [2 ]
Chen, Jinquan [2 ]
机构
[1] Beijing Univ Chinese Med, Beijing, Peoples R China
[2] Dongying Inspect Ctr Food & Drug, Beijing, Peoples R China
[3] Dongying Environm Protect Agcy, Beijing, Peoples R China
来源
JOURNAL OF CHROMATOGRAPHY B-ANALYTICAL TECHNOLOGIES IN THE BIOMEDICAL AND LIFE SCIENCES | 2016年 / 1025卷
关键词
Ion mobility spectrometry; Azo dye; Orange II; Allura red; Para red; PERFORMANCE LIQUID-CHROMATOGRAPHY; MASS-SPECTROMETRY; CAPILLARY-ELECTROPHORESIS; PHOTODIODE-ARRAY; SYNTHETIC DYES; SOFT DRINKS; MICROEXTRACTION; ADULTERATION; COLORANTS; SAMPLES;
D O I
10.1016/j.jchromb.2016.05.002
中图分类号
Q5 [生物化学];
学科分类号
071010 ; 081704 ;
摘要
Color is an important property for food evaluation. Synthetic azo dyes are usually used in food product to obtain better appearance because of their stability and low cost. However, such dyes should be strictly controlled because of their potential threat to human health. A simple, rapid and sensitive method has been developed to determine orange II, allura red, and para red simultaneously by ion mobility spectrometry. The three dyes could be separated at the same time and the migration time of orange II, allura red, and para red are 12.070 +/- 0.010, 8.180 +/- 0.015, and 11.037 +/- 0.016 ms, respectively. The effects of different parameters, such as pH, solvent, percentage of water, were investigated to establish the optimal condition. The detection limits were 0.1, 0.05, and 0.2 mu g/mL for orange II, allura red, and para red, respectively. The recoveries of the three azo dyes from jellies were all higher than 81%. The developed method is fast and accurate for the detection of the three synthetic dyes. (C) 2016 Elsevier B.V. All rights reserved.
引用
收藏
页码:105 / 109
页数:5
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