Study on the Timing of Degassing for Reproducible Preparation of Polymer-Based Monolithic Columns

被引：0
|
作者：
Ohyama, Kaname [1 ]
Sueyoshi, Tomoyuki [1 ]
Kishikawa, Naoya [1 ]
Nakashima, Kenichiro [2 ]
Kuroda, Naotaka [1 ]
机构：
[1] Nagasaki Univ, Grad Sch Biomed Sci, Dept Environm & Pharmaceut Sci, Nagasaki 8528521, Japan
[2] Nagasaki Univ, Grad Sch Biomed Sci, Dept Clin Pharm, Nagasaki 8528521, Japan
来源：
CHROMATOGRAPHIA | 2010年 / 71卷 / 9-10期
关键词：
Capillary electrochromatography; Polymer-based monolithic column; CAPILLARY ELECTROCHROMATOGRAPHY; LIQUID-CHROMATOGRAPHY; METHACRYLATE; OPTIMIZATION; SEPARATION;
D O I：
10.1365/s10337-010-1579-9
中图分类号：
Q5 [生物化学];
学科分类号：
071010 ; 081704 ;
摘要：
The influence of timing of degassing during the preparation procedure on reproducible preparation of polymer-based monolithic columns was investigated. The degassing of each solvent before preparing the polymerization mixture exhibited good reproducibility and was found to be appropriate for the monolithic column without any change in the composition of the polymerization mixture.
引用
收藏
页码：971 / 973
页数：3
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