Efficient heteronuclear dipolar decoupling in solid-state nuclear magnetic resonance at rotary resonance conditions

被引：10
|
作者：
Paul, Subhradip [2 ]
Mithu, Venus Singh [2 ]
Kurur, Narayanan D. [1 ]
Madhu, P. K. [2 ]
机构：
[1] Indian Inst Technol, Dept Chem, New Delhi 110016, India
[2] Tata Inst Fundamental Res, Dept Chem Sci, Bombay 400005, Maharashtra, India
来源：
JOURNAL OF MAGNETIC RESONANCE | 2010年 / 203卷 / 01期
关键词：
Solid-state NMR; Heteronuclear dipolar decoupling; Magic-angle spinning; TPPM; SPINAL; PISSARRO; Rotary resonance; ROTATING SOLIDS; CHEMICAL-SHIFT; ALPHA-GLYCINE; NMR; CRYSTALS;
D O I：
10.1016/j.jmr.2009.12.010
中图分类号：
Q5 [生物化学];
学科分类号：
071010 ; 081704 ;
摘要：
We introduce here a heteronuclear dipolar decoupling scheme in solid-state nuclear magnetic resonance that performs efficiently at the rotary resonance conditions. where otherwise dipolar couplings are reintroduced Results are shown proving the efficiency of this scheme at two magnetic fields under magic-angle spinning frequencies of 30 and 20 kHz (C) 2009 Elsevier Inc All rights reserved
引用
收藏
页码：199 / 202
页数：4
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