Synthesis and characterization of nano-sized zirconia powder synthesized by single emulsion-assisted direct precipitation

被引：84

作者：

Chandra, Navin ^{[1
]}

Singh, Deepesh Kumar ^{[1
]}

Sharma, Meenakshi ^{[1
]}

Upadhyay, Ravi Kant ^{[1
]}

Amritphale, S. S. ^{[1
]}

Sanghi, S. K. ^{[1
]}

机构：

[1] CSIR, Adv Mat & Proc Res Inst, Bhopal 462064, MP, India

来源：

JOURNAL OF COLLOID AND INTERFACE SCIENCE | 2010年 / 342卷 / 02期

关键词：

t-ZrO2; Phase transformation; Reverse microemulsion; X-ray diffraction (XRD); MICROEMULSION SYSTEM;

D O I：

10.1016/j.jcis.2009.10.065

中图分类号：

O64 [物理化学（理论化学）、化学物理学];

学科分类号：

070304 ; 081704 ;

摘要：

For the first time, single reverse microemulsion-assisted direct precipitation route has been successfully used to synthesize tetragonal zirconia nanoparticles in narrow size range. The synthesized powder was characterized using FT-IR, XRD and HRTEM techniques. The zirconia nanoparticles obtained were spherical in shape and has narrow particle size distribution in the range of 13-31 nm and crystallite size in the range of 13-23 nm. (C) 2009 Elsevier Inc. All rights reserved.

引用

页码：327 / 332

页数：6

共 21 条

[1] On the size-dependent phase transformation in nanoparticulate zirconia
Chraska, T
King, AH
Berndt, CC
[J]. MATERIALS SCIENCE AND ENGINEERING A-STRUCTURAL MATERIALS PROPERTIES MICROSTRUCTURE AND PROCESSING, 2000, 286 (01): : 169 - 178
[2] Hydrothermal synthesis of ZrO2-Y2O3 solid solutions at low temperature
Dell'Agli, G
Mascolo, G
[J]. JOURNAL OF THE EUROPEAN CERAMIC SOCIETY, 2000, 20 (02) : 139 - 145
[3] Water/span80/Triton X-100/n-hexyl alcohol/n-octane microemulsion system and the study of its application for preparing nanosized zirconia
Duan, GR
Yang, XJ
Huang, GH
Lu, LD
Wang, X
[J]. MATERIALS LETTERS, 2006, 60 (13-14) : 1582 - 1587
[4] Ultrafine zirconia powders via microemulsion processing route
Fang, JY
Wang, J
Ng, SC
Chew, CH
Gan, LM
[J]. NANOSTRUCTURED MATERIALS, 1997, 8 (04): : 499 - 505
[5] Atomic-scale structure of nanocrystalline ZrO2 prepared by high-energy ball milling -: art. no. 224107
Gateshki, M
Petkov, V
Williams, G
Pradhan, SK
Ren, Y
[J]. PHYSICAL REVIEW B, 2005, 71 (22)
[6] The surface structure of sulfated zirconia:: Periodic ab initio study of sulfuric acid adsorbed on ZrO2(101) and ZrO2(001)
Haase, F
Sauer, J
[J]. JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1998, 120 (51) : 13503 - 13512
[7] Preparation of spherical ultrafine zirconia powder in microemulsion system and its dispersibility
Huang, Y
Ma, T
Yang, JL
Zhang, LM
He, JT
Li, HF
[J]. CERAMICS INTERNATIONAL, 2004, 30 (05) : 675 - 681
[8] Stabilization of isolated hydrous amorphous and tetragonal zirconia nanoparticles through the formation of a passivating alumina shell
Kirsch, BL
Tolbert, SH
[J]. ADVANCED FUNCTIONAL MATERIALS, 2003, 13 (04) : 281 - 288
[9] SYNTHESIS OF FINE SPHERICAL ZIRCONIA PARTICLES BY CONTROLLED HYDROLYSIS OF ZIRCONIUM ALKOXIDE IN THE HIGH-TEMPERATURE RANGE ABOVE 50-DEGREES-C
KUMAZAWA, H
INOUE, T
SADA, E
[J]. CHEMICAL ENGINEERING JOURNAL AND THE BIOCHEMICAL ENGINEERING JOURNAL, 1994, 55 (1-2): : 93 - 96
[10] Characterization and synthesis of pure ZrO2 nanopowders via sonochemical method
Liang, JH
Jiang, X
Liu, G
Deng, ZX
Zhuang, J
Li, FL
Li, YD
[J]. MATERIALS RESEARCH BULLETIN, 2003, 38 (01) : 161 - 168

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