Synthesis and characterization of nano-sized zirconia powder synthesized by single emulsion-assisted direct precipitation

被引：85

作者：

Chandra, Navin ^{[1
]}

Singh, Deepesh Kumar ^{[1
]}

Sharma, Meenakshi ^{[1
]}

Upadhyay, Ravi Kant ^{[1
]}

Amritphale, S. S. ^{[1
]}

Sanghi, S. K. ^{[1
]}

机构：

[1] CSIR, Adv Mat & Proc Res Inst, Bhopal 462064, MP, India

来源：

JOURNAL OF COLLOID AND INTERFACE SCIENCE | 2010年 / 342卷 / 02期

关键词：

t-ZrO2; Phase transformation; Reverse microemulsion; X-ray diffraction (XRD); MICROEMULSION SYSTEM;

D O I：

10.1016/j.jcis.2009.10.065

中图分类号：

O64 [物理化学（理论化学）、化学物理学];

学科分类号：

070304 ; 081704 ;

摘要：

For the first time, single reverse microemulsion-assisted direct precipitation route has been successfully used to synthesize tetragonal zirconia nanoparticles in narrow size range. The synthesized powder was characterized using FT-IR, XRD and HRTEM techniques. The zirconia nanoparticles obtained were spherical in shape and has narrow particle size distribution in the range of 13-31 nm and crystallite size in the range of 13-23 nm. (C) 2009 Elsevier Inc. All rights reserved.

引用

页码：327 / 332

页数：6

共 21 条

[1] On the size-dependent phase transformation in nanoparticulate zirconia [J].

Chraska, T ;

King, AH ;

Berndt, CC .

MATERIALS SCIENCE AND ENGINEERING A-STRUCTURAL MATERIALS PROPERTIES MICROSTRUCTURE AND PROCESSING, 2000, 286 (01) :169-178

[2] Hydrothermal synthesis of ZrO2-Y2O3 solid solutions at low temperature [J].

Dell'Agli, G ;

Mascolo, G .

JOURNAL OF THE EUROPEAN CERAMIC SOCIETY, 2000, 20 (02) :139-145

[3] Water/span80/Triton X-100/n-hexyl alcohol/n-octane microemulsion system and the study of its application for preparing nanosized zirconia [J].

Duan, GR ;

Yang, XJ ;

Huang, GH ;

Lu, LD ;

Wang, X .

MATERIALS LETTERS, 2006, 60 (13-14) :1582-1587

[4] Ultrafine zirconia powders via microemulsion processing route [J].

Fang, JY ;

Wang, J ;

Ng, SC ;

Chew, CH ;

Gan, LM .

NANOSTRUCTURED MATERIALS, 1997, 8 (04) :499-505

[5] Atomic-scale structure of nanocrystalline ZrO2 prepared by high-energy ball milling -: art. no. 224107 [J].

Gateshki, M ;

Petkov, V ;

Williams, G ;

Pradhan, SK ;

Ren, Y .

PHYSICAL REVIEW B, 2005, 71 (22)

[6] The surface structure of sulfated zirconia:: Periodic ab initio study of sulfuric acid adsorbed on ZrO2(101) and ZrO2(001) [J].

Haase, F ;

Sauer, J .

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1998, 120 (51) :13503-13512

[7] Preparation of spherical ultrafine zirconia powder in microemulsion system and its dispersibility [J].

Huang, Y ;

Ma, T ;

Yang, JL ;

Zhang, LM ;

He, JT ;

Li, HF .

CERAMICS INTERNATIONAL, 2004, 30 (05) :675-681

[8] Stabilization of isolated hydrous amorphous and tetragonal zirconia nanoparticles through the formation of a passivating alumina shell [J].

Kirsch, BL ;

Tolbert, SH .

ADVANCED FUNCTIONAL MATERIALS, 2003, 13 (04) :281-288

[9] SYNTHESIS OF FINE SPHERICAL ZIRCONIA PARTICLES BY CONTROLLED HYDROLYSIS OF ZIRCONIUM ALKOXIDE IN THE HIGH-TEMPERATURE RANGE ABOVE 50-DEGREES-C [J].

KUMAZAWA, H ;

INOUE, T ;

SADA, E .

CHEMICAL ENGINEERING JOURNAL AND THE BIOCHEMICAL ENGINEERING JOURNAL, 1994, 55 (1-2) :93-96

[10] Characterization and synthesis of pure ZrO2 nanopowders via sonochemical method [J].

Liang, JH ;

Jiang, X ;

Liu, G ;

Deng, ZX ;

Zhuang, J ;

Li, FL ;

Li, YD .

MATERIALS RESEARCH BULLETIN, 2003, 38 (01) :161-168

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