Microwave-promoted solvent-free synthesis of para-quinone methides (p-QMs) derivatives

被引：7

作者：

Liu, Zhang-Qin ^{[1
]}

You, Peng-Sheng ^{[1
]}

Wu, Chuan-Hua ^{[1
]}

Han, Yang-Hong ^{[1
]}

机构：

[1] Southwest Univ, Coll Chem & Chem Engn, Key Lab Appl Chem Chongqing Municipal, Chongqing 400715, Peoples R China

来源：

JOURNAL OF SAUDI CHEMICAL SOCIETY | 2020年 / 24卷 / 01期

基金：

中国国家自然科学基金;

关键词：

Para-Quinone methides (p-QMs); Green chemistry; Microwave irradiation; Environment friendly synthesis; EFFICIENT;

D O I：

10.1016/j.jscs.2019.10.001

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

A rapid and efficient methodology for the synthesis of polysubstituted para-quinone methides (p-QMs) from aldehyde and 2,6-di-tert-butylphenol has been achieved in solvent-free and microwave irradiation condition within 33 min. This strategy displays the advantages including high atom economy, good functional group tolerance, and environmentally friendly operation. (C) 2019 King Saud University. Published by Elsevier B.V.

引用

页码：120 / 126

页数：7

共 41 条

[1] Microwave assisted synthesis of substituted furan-2-carboxaldehydes and their reactions [J].

Al-Hazimi, Hassan M. A. ;

Al-Alshaikh, Monirah A. .

JOURNAL OF SAUDI CHEMICAL SOCIETY, 2010, 14 (04) :373-382

[2] Dibenzal acetone and triphenyl methane. [J].

Baeyer, A ;

Villiger, V .

BERICHTE DER DEUTSCHEN CHEMISCHEN GESELLSCHAFT, 1903, 36 :2774-2796

[3] Neocandenatone, an isoflavan-cinnamylphenol quinone methide pigment from Dalbergia congestiflora [J].

Barragán-Huerta, BE ;

Peralta-Cruz, J ;

González-Laredo, RF ;

Karchesy, J .

PHYTOCHEMISTRY, 2004, 65 (07) :925-928

[4] Synthesis of 2,4,5-triarylated imidazoles via three-component domino reaction under catalyst-free conditions [J].

Chen, Yang ;

Wang, Ren ;

Ba, Feifei ;

Hou, Junli ;

Ding, Aishun ;

Zhou, Mingdong ;

Guo, Hao .

JOURNAL OF SAUDI CHEMICAL SOCIETY, 2017, 21 (01) :76-81

[5] A microwave-assisted facile synthesis of novel coumarin derivatives containing cyanopyridine and furan as antimicrobial agents [J].

Desai, N. C. ;

Satodiya, H. M. ;

Rajpara, K. M. ;

Joshi, V. V. ;

Vaghani, H. V. .

JOURNAL OF SAUDI CHEMICAL SOCIETY, 2017, 21 :S153-S162

[6] ELECTROORGANIC REACTIONS .31. QUINONEMETHIDE RADICAL-ANIONS AND DIANIONS - THEIR CATHODIC GENERATION AND REACTIVITY [J].

GOULART, MOF ;

UTLEY, JHP .

JOURNAL OF ORGANIC CHEMISTRY, 1988, 53 (11) :2520-2525

[7] A highly diastereoselective [5+1] annulation to 2,2,3-trisubstituted tetrahydroquinoxalines via intramolecular Mannich-type trapping of ammonium ylides [J].

Guan, Xiao-Yu ;

Tang, Min ;

Liu, Zhang-Qin ;

Hu, WenHao .

CHEMICAL COMMUNICATIONS, 2019, 55 (66) :9809-9812

[8] 1,6-Conjugate sulfonylation of para-quinone methides: An expedient approach to unsymmetrical gem-diarylmethyl sulfones [J].

Guan, Xiao-Yu ;

Zhang, Liang-Dong ;

You, Peng-Sheng ;

Liu, Sheng-Shu ;

Liu, Zhang-Qin .

TETRAHEDRON LETTERS, 2019, 60 (03) :244-247

[9] Efficient and selective α-bromination of carbonyl compounds with N-bromosuccinimide under microwave [J].

Guan, Xiao-Yu ;

Al-Misba'a, Zahra ;

Huang, Kuo-Wei .

ARABIAN JOURNAL OF CHEMISTRY, 2015, 8 (06) :892-896

[10] Near-Infrared Fluorescent Rosol Dye Tailored toward Lymphatic Mapping Applications [J].

Hettie, Kenneth S. ;

Klockow, Jessica L. ;

Glass, Timothy E. ;

Chin, Frederick T. .

ANALYTICAL CHEMISTRY, 2019, 91 (04) :3110-3117

← 1 2 3 4 5 →