Investigation on the preparation and properties of monodispersed Al2O3-ZrO2 nanopowder via Co-precipitation method

被引:16
作者
Zhou, Mei [1 ]
Xu, Linfeng [1 ]
Xi, Xiuan [2 ]
Li, Ping [3 ]
Dai, Wubin [1 ]
Zhu, Wenli [1 ]
Shui, Anze [1 ]
Zeng, Lingke [1 ]
机构
[1] S China Univ Technol, Sch Mat Sci & Engn, Guangzhou 510640, Guangdong, Peoples R China
[2] Osaka Univ, Joining & Welding Res Inst, 11-1 Mihogaoka, Osaka 5670047, Japan
[3] Chinese Acad Sci, Guangzhou Inst Energy Convers, Guangzhou 510640, Guangdong, Peoples R China
基金
中国博士后科学基金;
关键词
Nanopowder; Monodisperse; Co-precipitation; Al2O3-ZrO4; Relative density; MECHANICAL-PROPERTIES; ZIRCONIA; ALUMINA; MICROSTRUCTURE; DISSOLUTION; SOLUBILITY;
D O I
10.1016/j.jallcom.2016.03.265
中图分类号
O64 [物理化学(理论化学)、化学物理学];
学科分类号
070304 ; 081704 ;
摘要
With Al2O3 as inhibitor (which can be etched after calcination), monodispersed Al2O3-ZrO2 nanopowder was successful prepared by co-precipitation method. The as-prepared powders were characterized by acoustic particle sizer (APS), SEM, TEM and XRD, respectively. Crystalline and non-agglomerated nanometric Al2O3-ZrO2 powders with very small crystallite size (similar to 7 nm) and narrow size distribution can be obtained. The relative yield was effected dramatically by pH and the ratio of M-AHC: M-Zr. Green bodies have an ultrafine uniform microstructure without apparent macropore through 200 MPa CIP treatment. The relative density of the grains can be reached to similar to 98.2% by sintering at 1050 degrees C for 4 h, with an average grain size degrees 39 nm. (C) 2016 Elsevier B.V. All rights reserved.
引用
收藏
页码:337 / 342
页数:6
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