7-Benzenesulfonamido-3-methyl-8-oxo-5-thia-1-azabicyclo[4.2.0]octa-2-ene-2-carboxylic acid monohydrate

被引：3

作者：

Sharif, Shahzad ^{[2
]}

Akkurt, Mehmet ^{[1
]}

Khan, Islam Ullah ^{[2
]}

Salariya, Manan Ayub ^{[3
]}

Ahmad, Sarfraz ^{[3
]}

机构：

[1] Erciyes Univ, Dept Phys, Fac Arts & Sci, TR-38039 Kayseri, Turkey

[2] Govt Coll Univ, Dept Chem, Mat Chem Lab, Lahore 54000, Pakistan

[3] Pharmagen Ltd, Lahore 54000, Pakistan

来源：

ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE | 2010年 / 66卷

关键词：

D O I：

10.1107/S1600536809051769

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

In the title compound, C14H14N2O5S2 center dot H2O, the six-membered ring fused to the beta-lactam unit has a twisted conformation. Weak intramolecular N-H center dot center dot center dot S and C-H center dot center dot center dot O interactions occur. Intermolecular C-H center dot center dot center dot S, N-H center dot center dot center dot O, C-H center dot center dot center dot O and O-H center dot center dot center dot O hydrogen-bonding interactions stabilize the crystal structure, forming a three-dimensional network. Weak C-H center dot center dot center dot pi interactions are also present.

引用

页码：O73 / U1695

页数：13

共 50 条

[31] Crystal structure of (1α,2β,8α)-2-methyl-8-phenyl-2-azabicyclo[4.2.0]oct-5-ene(N-B)boran, (C6H5)C7H9N(CH3)(BH3)
Peters, EM
Peters, K
Groetsch, S
Christl, M
ZEITSCHRIFT FUR KRISTALLOGRAPHIE-NEW CRYSTAL STRUCTURES, 2001, 216 (01): : 121 - 122
[32] Synthesis and Crystal Structure of 2-Fluoro-4-methyl-3-oxo-4-aza-5α-androst-1-ene-17β-carboxylic Acid Methyl Ester
Jang Yin-Zhi
Xiang Zuo
Liang Da-Wei
CHINESE JOURNAL OF STRUCTURAL CHEMISTRY, 2010, 29 (04) : 509 - 514
[33] Synthesis and Crystal Structure of 2-Fluoro-4-methyl-3-oxo-4-aza-5α-androst-1-ene-17β-carboxylic Acid Methyl Ester
江银枝
项卓
梁大伟
结构化学, 2010, 29 (04) : 509 - 514
[34] 7-OXO-2-THIA-1-AZABICYCLO[3.2.0]HEPT-3-ENE - REVISED STRUCTURE FOR PENEMS SYNTHESIZED VIA OXIDATIVE ADDITION MEDIATED BY COPPER(I)
OIDA, S
YOSHIDA, A
HAYASHI, T
NAKAYAMA, E
SATO, S
OHKI, E
TETRAHEDRON LETTERS, 1980, 21 (07) : 619 - 620
[35] (6R,7R)-7-[(R)-2-CARBOXY-2-(4-HYDROXYPHENYL)ACETAMIDO]-7-METHOXY-3-[[(1-METHYL-1H-TETRAZOL-5-YL)THIO]METHYL]-8-OXO-5-OXA-1-AZABICYCLO[4.2.0]OCT-2-ENE-2-CARBOXYLIC ACID DIAMMONIUM SALT 9/2 HYDRATE, C20H18N6O9S.2NH4.9/2H2O
SHIRO, M
NAKAI, H
MATSUBARA, F
KIKKAWA, I
CRYSTAL STRUCTURE COMMUNICATIONS, 1982, 11 (02): : 727 - 732
[36] SYNTHESIS OF 7-OXO-1-AZABICYCLO[3.2.0]HEPT-2-ENE-2-CARBOXYLATES - OLIVANIC ACID RING-SYSTEM
BAXTER, AJG
DICKINSON, KH
ROBERTS, PM
SMALE, TC
SOUTHGATE, R
JOURNAL OF THE CHEMICAL SOCIETY-CHEMICAL COMMUNICATIONS, 1979, (05) : 236 - 237
[37] 3-methyl-4-oxo-2-phenyl-4H-chromene-8-carboxylic acid
Hong, Zhi
Jiang, Hua-Jiang
Zhuang, Yu-Guo
Guo, Hai-Chang
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2008, 64 : O857 - U1868
[38] DERIVATION OF 3-OXAZOLIN-5-ONES FROM METHYL (4S,6S)-5,5,9,9-TETRAMETHYL-7-OXO-8-OXA-4-THIA-1-AZABICYCLO[4,3,0]NON-2-ENE-3-CARBOXYLATE 4-OXIDE
STOODLEY, RJ
WILKINS, RB
JOURNAL OF THE CHEMICAL SOCIETY-CHEMICAL COMMUNICATIONS, 1974, (19) : 796 - 797
[39] Benzothiazol-2-amine-3-methoxycarbonyl-7-oxabicyclo[2.2.1]hept-5-ene-2-carboxylic acid (1/1)
Li, Jian
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2011, 67 : O199 - U3115
[40] AN EFFICIENT SYTHESIS OF (+/-) 7-OXO-3-THIA-1-AZABICYCLO[3.2.0]HEPTANE-2-CARBOXYLATE-3,3-DIOXIDE
BRENNAN, J
PINTO, IL
TETRAHEDRON LETTERS, 1983, 24 (43) : 4731 - 4732

← 1 2 3 4 5 →