Carbon ceramic nanoparticulate film electrode prepared from oppositely charged particles by layer-by-layer approach

被引：23
|
作者：
Lesniewski, Adam [1 ]
Niedziolka-Jonsson, Joanna [1 ]
Rizzi, Cecile [2 ,3 ]
Gaillon, Laurent [2 ,3 ]
Rogalski, Jerzy [4 ]
Opallo, Marcin [1 ,5 ]
机构：
[1] Polish Acad Sci, Inst Phys Chem, PL-01224 Warsaw, Poland
[2] Univ Paris 06, UPMC, UMR 7195, Lab Physicochim Eletrolytes Colloides & Sci Analy, F-75005 Paris, France
[3] ESPCI, UMR 7195, F-75005 Paris, France
[4] Marie Curie Sklodowska Univ, Dept Biochem, PL-20031 Lublin, Poland
[5] Univ Cardinal Stefan Wyszynski, Fac Math & Nat Sci, Coll Sci, Warsaw, Poland
来源：
ELECTROCHEMISTRY COMMUNICATIONS | 2010年 / 12卷 / 01期
关键词：
Carbon ceramic electrode; Layer-by-layer; Carbon nanoparticles; Silicate particles; Laccase; MULTILAYER FILMS; IONIC LIQUID; SILICA; GOLD; ACCUMULATION;
D O I：
10.1016/j.elecom.2009.10.041
中图分类号：
O646 [电化学、电解、磁化学];
学科分类号：
081704 ;
摘要：
Carbon ceramic nanoparticulate film electrode was prepared from negatively charged sulfonated carbon nanoparticles and positively charged silicate submicrometre particles with appended imidazolium groups. They were immobilized on an indium tin oxide surface by layer-by-layer method: alternative immersion into suspension of positive and negative particles. The film formation is confirmed by scanning electron microscopy - after larger number of immersion and withdrawal steps more material is deposited on the electrode substrate. The nanoparticulate film is stable and the obtained electrode exhibits a significant increase of capacitive current and faradaic current corresponding to hydrogen peroxide electroreduction. The effect of the number of immersion and withdrawal steps is strikingly visible on dioxygen bioelectrocatalytic reduction current after adsorption of the enzyme laccase. (C) 2009 Elsevier B.V. All rights reserved.
引用
收藏
页码：83 / 85
页数：3
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