Improved quality and functional properties of Ti-6Al-4V ELI alloy for personalized orthopedic implants fabrication with EBM process

被引:26
作者
Szymczyk-Ziolkowska, Patrycja [1 ]
Ziolkowski, Grzegorz [1 ]
Hoppe, Viktoria [1 ]
Rusinska, Malgorzata [1 ]
Kobiela, Karol [1 ]
Madeja, Marcin [1 ]
Dziedzic, Robert [1 ]
Junka, Adam [2 ]
Detyna, Jerzy [3 ]
机构
[1] Wroclaw Univ Sci & Technol, Fac Mech Engn, Fraunhofer Project Ctr, Ctr Adv Mfg Technol, Lukasiewicza 5, PL-50371 Wroclaw, Poland
[2] Wroclaw Med Univ, Dept Pharmaceut Microbiol & Parasitol, PL-50556 Wroclaw, Poland
[3] Wroclaw Univ Sci & Technol, Fac Mech Engn, Dept Mech Mat & Biomed Engn, Wroclaw, Poland
关键词
Additive manufacturing; EBM; Process parameters; HIP; XCT; SEM; XRD; Mechanical properties; Cytotoxicity; Personalized jaw implants; BEAM MELTING EBM; MECHANICAL-PROPERTIES; SURFACE-ROUGHNESS; ADDITIVE MANUFACTURE; TITANIUM-ALLOYS; BONE INGROWTH; ELECTRON; MICROSTRUCTURE; LASER; METAL;
D O I
10.1016/j.jmapro.2022.02.011
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
Understanding the manufacturing process parameters and their correlation with final product functional properties is needed to ensure performance in critical applications in the medical industry. This article presents the holistic procedure for verifying the quality of manufactured products, including the determination of basic material characteristics and strength parameters based on EBM (Electron Beam Melting) technology for the titanium alloy Ti-6Al-4V ELI. The aim of this study was to investigate the effects of the manufacturing and post processing methods used, on the geometric accuracy, microstructure, mechanical and cytotoxic properties of additively manufactured parts, especially in the form of personalized jaw implants. The effect of Hot Isostatic Pressing (HIP) treatment on microstructure and properties is also taken into account. The EBM manufacturing process was developed and samples were built using three different orientations: 0?degrees (horizontally), 45?degrees (diagonally), and 90?degrees (vertically). The novel results are systematically presented and discussed beginning from the selection of process parameters, sample manufacturing, wide microstructural characterization, determination of static mechanical properties as well as geometric accuracy, and quality control verification depending on the manufacturing process and the post-processing methods used. The conducted research allowed for the presentation of the entire process chain of the EBM manufactured medical implant made of high-purity titanium alloy (Ti-6Al-4V ELI), thus filling the scientific gaps related to the selective presentation and discussion of research results published in the literature on the subject.
引用
收藏
页码:175 / 194
页数:20
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