Influence of aluminium nitride as a foaming agent on the preparation of foam glass-ceramics from high-titanium blast furnace slag

被引:34
作者
Shi, Huan [1 ]
Feng, Ke-qin [1 ]
Wang, Hai-bo [1 ,2 ]
Chen, Chang-hong [1 ]
Zhou, Hong-ling [1 ]
机构
[1] Sichuan Univ, Sch Mfg Sci & Engn, Chengdu 610065, Peoples R China
[2] Panzhihua Coll, Sch Mat Engn, Panzhihua 617000, Peoples R China
关键词
blast furnace slag; aluminium nitride; powder sintering; foam; glass-ceramics; crystallization; CRYSTALLIZATION BEHAVIOR; WASTE GLASS; TIO2; MICROSTRUCTURE; RECOVERY; RATIO; ASH;
D O I
10.1007/s12613-016-1271-7
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
To effectively reuse high-titanium blast furnace slag (TS), foam glass-ceramics were successfully prepared by powder sintering at 1000A degrees C. TS and waste glass were used as the main raw materials, aluminium nitride (AlN) as the foaming agent, and borax as the fluxing agent. The influence of the amount of AlN added (1wt%-5wt%) on the crystalline phases, microstructure, and properties of the produced foam glass-ceramics was studied. The results showed that the main crystal phases were perovskite, diopside, and augite. With increasing AlN content, a transformation from diopside to augite occurred and the crystallinity of the pyroxene phases slightly decreased. Initially, the average pore size and porosity of the foam glass-ceramics increased and subsequently decreased; similarly, their bulk density and compressive strength decreased and subsequently increased. The optimal properties were obtained when the foam glass-ceramics were prepared by adding 4wt% AlN.
引用
收藏
页码:595 / 600
页数:6
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