Energy calibration and intensity normalization in high-resolution NEXAFS spectroscopy

被引：69

作者：

Schöll, A ^{[1
]}

Zou, Y ^{[1
]}

Schmidt, T ^{[1
]}

Fink, R ^{[1
]}

Umbach, E ^{[1
]}

机构：

[1] Univ Wurzburg, D-97074 Wurzburg, Germany

来源：

JOURNAL OF ELECTRON SPECTROSCOPY AND RELATED PHENOMENA | 2003年 / 129卷 / 01期

关键词：

NEXAFS; calibration; normalization; carbon edge;

D O I：

10.1016/S0368-2048(03)00016-1

中图分类号：

O433 [光谱学];

学科分类号：

0703 ; 070302 ;

摘要：

Using high-brilliance synchrotron radiation and an ultrahigh-resolution monochromator a wealth of new fine structures can be observed in near-edge X-ray absorption spectra. The potential information gain, however, requires an accurate calibration of the energy scale and a perfect intensity normalization in order to avoid erroneous results, e.g., the occurrence of spurious peaks. By means of the most problematic C 1s edge it is shown how large these effects can be and how appropriate energy calibration and intensity normalization can be achieved. (C) 2003 Elsevier Science B.V. All rights reserved.

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页码：1 / 8

页数：8

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