Solvothermal synthesis of molybdenum disulfide hollow spheres modified by cyanex 301 in water-ethanol medium

被引:11
作者
Fu, Xun [1 ]
Wu, Danmei [1 ]
Zhou, Xiaodong [1 ]
Shi, Huaqiang [1 ]
Hu, Zhengshui [1 ]
机构
[1] Qingdao Univ Sci & Technol, Shandong 266042, Peoples R China
关键词
molybdenum disulfide; hollow spheres; solvothermal synthesis; nanoparticles; colloids;
D O I
10.1007/s11051-006-9120-7
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
Hollow spherical molybdenum disulfide has been successfully synthesized via a solvothermal method using Cyanex 301 as sulfur source and modification agent. The hollow spheres are characterized by transmission electron microscopy, scanning electron microscopy, X-ray diffraction and Energy-Dispersive X-ray analysis. The influences of reaction conditions are also discussed while a mechanism is proposed to explain the formation of the peculiar morphology.
引用
收藏
页码:675 / 681
页数:7
相关论文
共 15 条
[11]  
SHI HQ, IN PESS J SOLID STAT
[12]   COBALT NICKEL SEPARATION - THE EXTRACTION OF COBALT(II) AND NICKEL(II) BY CYANEX-301, CYANEX-302 AND CYANEX-272 [J].
TAIT, BK .
HYDROMETALLURGY, 1993, 32 (03) :365-372
[15]   Low temperature synthesis and characterization of molybdenum disulfide nanotubes and nanorods [J].
Tian, Y ;
He, Y ;
Zhu, YF .
MATERIALS CHEMISTRY AND PHYSICS, 2004, 87 (01) :87-90