Preparation of Co2+-doped ZnAl2O4 nanoparticles by citrate sol-gel method

被引：58

作者：

Duan, XL ^{[1
]}

Yuan, DR ^{[1
]}

Sun, ZH ^{[1
]}

Luan, CN ^{[1
]}

Pan, DY ^{[1
]}

Xu, D ^{[1
]}

Lv, MK ^{[1
]}

机构：

[1] Shandong Univ, State Key Lab Crystal Mat, Jinan 250100, Peoples R China

来源：

JOURNAL OF ALLOYS AND COMPOUNDS | 2005年 / 386卷 / 1-2期

基金：

中国国家自然科学基金;

关键词：

nanostructures; sol-gel synthesis; x-ray diffraction; luminescence;

D O I：

10.1016/j.jallcom.2004.05.059

中图分类号：

O64 [物理化学（理论化学）、化学物理学];

学科分类号：

070304 ; 081704 ;

摘要：

Nano-sized ZnAl2O4 particles doped with Co2+ ions were prepared by a citrate sol-gel method. The precursor was prepared from metal nitrates and citric acid and heat-treated at 600-900degreesC. The nanocrystalline Co2+:ZnAl2O4 is characterized by X-ray diffraction transmission electron microscopy and luminescence spectroscopy. The precursor gel began to crystallize to the ZnAl2O4 nanopowders at 600degreesC. The average particles size was estimated as 16-30 nm in the temperature range of 600-900degreesC. The emission spectra of Co2+ZnAl2O4 in the visible region were characterized by the tetrahedrally coordinated Co2+. (C) 2004 Elsevier B.V. All rights reserved.

引用

页码：311 / 314

页数：4

共 12 条

[1] Low-temperature preparation of nanocrystalline lead zirconate titanate and lead lanthanum zirconate titanate powders using triethanolamine [J].

Das, RN ;

Pathak, A ;

Pramanik, P .

JOURNAL OF THE AMERICAN CERAMIC SOCIETY, 1998, 81 (12) :3357-3360

[2] LUMINESCENCE FROM LIGA5O8-CO [J].

DONEGAN, JF ;

BERGIN, FJ ;

IMBUSCH, GF ;

REMEIKA, JP .

JOURNAL OF LUMINESCENCE, 1984, 31-2 (DEC) :278-280

[3] Spectroscopic properties of Co2+: ZnAl2O4 nanocrystals in sol-gel derived glass-ceramics [J].

Duan, XL ;

Yuan, DR ;

Cheng, XF ;

Sun, ZH ;

Sun, HQ ;

Xu, D ;

Lv, MK .

JOURNAL OF PHYSICS AND CHEMISTRY OF SOLIDS, 2003, 64 (06) :1021-1025

[4]

EDELSTEIN A, 1996, CAMMARATA NANOMETERI

[5] ABSORPTION AND LUMINESCENCE OF TETRAHEDRAL CO2+ ION IN MGAL2O4 [J].

KULESHOV, NV ;

MIKHAILOV, VP ;

SCHERBITSKY, VG ;

PROKOSHIN, PV ;

YUMASHEV, KV .

JOURNAL OF LUMINESCENCE, 1993, 55 (5-6) :265-269

[6] 72 W Nd:Y3Al5O12 ceramic laser [J].

Lu, JR ;

Murai, T ;

Takaichi, K ;

Uematsu, T ;

Misawa, K ;

Prabhu, M ;

Xu, J ;

Ueda, K ;

Yagi, H ;

Yanagitani, T ;

Kaminskii, AA ;

Kudryashov, A .

APPLIED PHYSICS LETTERS, 2001, 78 (23) :3586-3588

[7]

Okhrimchuk A.G., 1998, ADV SOLID STATE LASE, V19, P185, DOI [10.1364/ASSL.1998.LS9, DOI 10.1364/ASSL.1998.LS9]

[8] Synthesis of nanoparticle of inorganic oxides by polymer matrix [J].

Pramanik, P .

BULLETIN OF MATERIALS SCIENCE, 1995, 18 (06) :819-829

[9] An improved synthesis method for indenes and styrenes by use of a ZnO/Al2O3 spinel catalyst [J].

Roesky, R ;

Weiguny, J ;

Bestgen, H ;

Dingerdissen, U .

APPLIED CATALYSIS A-GENERAL, 1999, 176 (02) :213-220

[10] PREPARATION AND PROPERTIES OF FINE PARTICLE NICKEL ZINC FERRITES - A COMPARATIVE-STUDY OF COMBUSTION AND PRECURSOR METHODS [J].

SURESH, K ;

PATIL, KC .

JOURNAL OF SOLID STATE CHEMISTRY, 1992, 99 (01) :12-17

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