Crystal structure of tris{2,2′-[1,2-[methylenebis(thio)]-bis[1,3,4-thiadiazole]]}copper(II) tetranitrate - acetonitrile (1:1), Cu2(C5H4N4S4)3(NO3)4•CH3CN

被引:0
作者
Qin, Jian-Hua [1 ]
Hu, Pu-Zhou [1 ]
机构
[1] Luoyang Normal Univ, Coll Chem & Chem Engn, Luoyang 471022, Henan, Peoples R China
来源
ZEITSCHRIFT FUR KRISTALLOGRAPHIE-NEW CRYSTAL STRUCTURES | 2010年 / 225卷 / 01期
关键词
MAGNETIC-PROPERTIES; COMPLEXES;
D O I
10.1524/ncrs.2010.0024
中图分类号
O7 [晶体学];
学科分类号
0702 ; 070205 ; 0703 ; 080501 ;
摘要
C17H15Cu2N17O12S12, triclinic, P (1) over bar (no. 2), a = 10.8052(7) angstrom, b = 12 2282(8) angstrom, c = 16.927(1) angstrom, alpha = 85 757(1)degrees, beta = 78.075(1)degrees, gamma = 70.174(1)degrees, V = 2058 5 angstrom(3), Z = 2, R-gt(F) = 0.030, wR(ref)(F-2) = 0.077, T = 291 K
引用
收藏
页码:60 / 62
页数:3
相关论文
共 10 条
[1]   SYNTHESIS, CRYSTAL AND MOLECULAR-STRUCTURE AND MAGNETIC-PROPERTIES OF BIS[(MU-HYDROXO)BIS(MU-2,5-DIAMINO-1,3,4-THIADIAZOLE-N-1, N-2-CHLOROAQUA(2,5-DIAMINO-1,3,4-THIADIAZOLE-N-1)COBALT(II)-O,N-1, N-1]-COBALT(II) DICHLORIDE DIHYDRATE [J].
FABRETTI, AC ;
MALAVASI, W ;
GATTESCHI, D ;
SESSOLI, R .
INORGANICA CHIMICA ACTA, 1992, 195 (02) :157-161
[2]   SYNTHESIS AND CHARACTERIZATION OF COPPER(II) ACETAZOLAMIDE (5-ACETAMIDO-1,3,4-THIADIAZOLE-2-SULFONAMIDE) COMPLEXES - CRYSTAL-STRUCTURE OF DIMERIC [CU(ACM)(NH3)2(OH2)]2.2H2O [J].
FERRER, S ;
BORRAS, J ;
MIRATVILLES, C ;
FUERTES, A .
INORGANIC CHEMISTRY, 1990, 29 (02) :206-210
[3]   Probing the frameworks of polymeric of silver(I) nitrate complexes with flexible bisthiadiazole alkanes by tuning the ligand spacers [J].
Hu, Pu-Zhou ;
Wang, Jian-Ge ;
Ma, Lu-Fang ;
Qin, Jian-Hua ;
Zhao, Bang-Tun ;
Wang, Li-Ya .
JOURNAL OF MOLECULAR STRUCTURE, 2008, 876 (1-3) :225-233
[4]   Hydrothermal synthesis and magnetic behavior of a novel layered coordination polymer generated from manganese(II) adipate [J].
Kim, Y ;
Jung, DP .
INORGANIC CHEMISTRY, 2000, 39 (07) :1470-1475
[5]   Synthesis and crystal structure of tetranuclear copper(I) and silver(I) complexes bridged by 2-amino-1,3,4-thiadiazole (atdz):: [Cu4(atdz)6](ClO4)4 • 2CH3OH and [Ag4(atdz)6](ClO4)4 [J].
Maekawa, M ;
Munakata, M ;
Kuroda-Sowa, T ;
Suenaga, Y ;
Sugimoto, K .
INORGANICA CHIMICA ACTA, 1999, 290 (02) :153-158
[6]  
Sheldrick G.M., 2000, SHELXTL VERSION 614
[7]  
SHELDRICK GM, 1997, SHELXLS 97 PROGRAM R
[8]   [Cu(H4C3N2S)Cl2]n, an unprecedented diazole-bridged one-dimensional copper halide:: Synthesis, structure, and magnetic properties [J].
Song, JL ;
Dong, ZC ;
Zeng, HY ;
Zhou, WB ;
Naka, T ;
Wei, Q ;
Mao, JG ;
Guo, GC ;
Huang, JS .
INORGANIC CHEMISTRY, 2003, 42 (06) :2136-2140
[9]   Tetrakis(2-hydroxyphenyl)ethene and derivatives. A structurally preorganized tetradentate ligand system for polymetallic coordination chemistry and catalysis [J].
Verkerk, U ;
Fujita, M ;
Dzwiniel, TL ;
McDonald, R ;
Stryker, JM .
JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 2002, 124 (34) :9988-9989
[10]   Syntheses, structures, photoluminescence, and theoretical studies of d10 metal complexes of 2,2′-dihydroxy-[1,1′]binaphthalenyl-3,3′-dicarboxylate [J].
Zheng, SL ;
Yang, JH ;
Yu, XL ;
Chen, XM ;
Wong, WT .
INORGANIC CHEMISTRY, 2004, 43 (02) :830-838