3D electron diffraction of mono- and few-layer MoS2

被引:8
作者
Gorelik, Tatiana E. [1 ]
Nergis, Berkin [1 ,2 ]
Schoener, Tobias [1 ,3 ]
Koester, Janis [1 ]
Kaiser, Ute [1 ]
机构
[1] Ulm Univ, Cent Facil Elect Microscopy, Electron Microscopy Mat Sci EMMS, Albert Einstein Allee 11, D-89081 Ulm, Germany
[2] Karlsruhe Inst Technol, Inst Photon Sci & Synchrotron Radiat, 76344 Eggenstein Leopoldshafen, Hermann von Helmholtz Pl 1, D-76344 Eggenstein Leopoldshafen, Germany
[3] Tech Univ Munich, Arcisstr 21, D-80333 Munich, Germany
关键词
2D crystals; 3D electron diffraction; MoS2; TRANSITION-METAL DICHALCOGENIDES; 2-DIMENSIONAL MATERIALS;
D O I
10.1016/j.micron.2021.103071
中图分类号
TH742 [显微镜];
学科分类号
摘要
Mono-and few-layer MoS2 were studied by three-dimensional electron diffraction (3D ED) showing distinctly different symmetry for crystals consisting of odd and even number of layers. Experimentally obtained intensity distributions along the relrods match qualitatively kinematically simulated data. Our findings allow to differentiate unambiguously between 1-, 2-, 3- 4-and 5-layers MoS2 crystals.
引用
收藏
页数:11
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共 28 条
[1]   Ripples and Layers in Ultrathin MoS2 Membranes [J].
Brivio, Jacopo ;
Alexander, Duncan T. L. ;
Kis, Andras .
NANO LETTERS, 2011, 11 (12) :5148-5153
[2]   Recent development of two-dimensional transition metal dichalcogenides and their applications [J].
Choi, Wonbong ;
Choudhary, Nitin ;
Han, Gang Hee ;
Park, Juhong ;
Akinwande, Deji ;
Lee, Young Hee .
MATERIALS TODAY, 2017, 20 (03) :116-130
[3]   RELATIVISTIC CALCULATION OF ANOMALOUS SCATTERING FACTORS FOR X-RAYS [J].
CROMER, DT ;
LIBERMAN, D .
JOURNAL OF CHEMICAL PHYSICS, 1970, 53 (05) :1891-&
[4]   Beyond Graphene: Progress in Novel Two-Dimensional Materials and van der Waals Solids [J].
Das, Saptarshi ;
Robinson, Joshua A. ;
Dubey, Madan ;
Terrones, Humberto ;
Terrones, Mauricio .
ANNUAL REVIEW OF MATERIALS RESEARCH, VOL 45, 2015, 45 :1-27
[5]   Imaging Polarity in Two Dimensional Materials by Breaking Friedel's Law [J].
Deb, Pratiti ;
Cao, Michael C. ;
Han, Yimo ;
Holtz, Megan E. ;
Xie, Saien ;
Park, Jiwoong ;
Hovden, Robert ;
Muller, David A. .
ULTRAMICROSCOPY, 2020, 215
[6]   The crystal structure of molybdenite [J].
Dickinson, RG ;
Pauling, L .
JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1923, 45 :1466-1471
[7]   3D Electron Diffraction: The Nanocrystallography Revolution [J].
Gemmi, Mauro ;
Mugnaioli, Enrico ;
Gorelik, Tatiana E. ;
Kolb, Ute ;
Palatinus, Lukas ;
Boullay, Philippe ;
Hovmoller, Sven ;
Abrahams, Jan Pieter .
ACS CENTRAL SCIENCE, 2019, 5 (08) :1315-1329
[8]   The Rise of MXenes [J].
Gogotsi, Yury ;
Anasori, Babak .
ACS NANO, 2019, 13 (08) :8491-8494
[9]   Towards quantitative treatment of electron pair distribution function [J].
Gorelik, Tatiana E. ;
Neder, Reinhard ;
Terban, Maxwell W. ;
Lee, Zhongbo ;
Mu, Xiaoke ;
Jung, Christoph ;
Jacob, Timo ;
Kaiser, Ute .
ACTA CRYSTALLOGRAPHICA SECTION B-STRUCTURAL SCIENCE CRYSTAL ENGINEERING AND MATERIALS, 2019, 75 :532-549
[10]   Measuring the corrugation amplitude of suspended and supported graphene [J].
Kirilenko, D. A. ;
Dideykin, A. T. ;
Van Tendeloo, G. .
PHYSICAL REVIEW B, 2011, 84 (23)