Synthesis and characterization of spinel FeAl2O4 (hercynite) magnetic nanoparticles and their application in multicomponent reactions

被引：126
|
作者：
Ghorbani-Choghamarani, Arash [1 ]
Mohammadi, Masoud [1 ]
Shiri, Lotfi [1 ]
Taherinia, Zahra [1 ]
机构：
[1] Ilam Univ, Fac Sci, Dept Chem, POB 69315516, Ilam, Iran
来源：
RESEARCH ON CHEMICAL INTERMEDIATES | 2019年 / 45卷 / 11期
关键词：
FeAl2O4; Hercynite; Magnetic nanoparticles; Benzo[a]pyrano[2; 3-c] phenazine; Polyhydroquinoline; SEQUENTIAL 4-COMPONENT SYNTHESIS; ONE-POT SYNTHESIS; POLYHYDROQUINOLINE DERIVATIVES; IONIC LIQUID; ANTITUMOR-ACTIVITY; GREEN SYNTHESIS; EFFICIENT; CATALYST; NANOCATALYST; FERRITES;
D O I：
10.1007/s11164-019-03930-0
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
The spinel ferrite FeAl2O4 (hercynite) MNPs (magnetic nanoparticles) were applied as a reusable catalytic system for the one-pot synthesis of benzo[a]pyrano[2,3-c] phenazine and polyhydroquinoline derivatives via a multicomponent reaction under green reaction conditions. The structure of the prepared nanocatalyst has been characterized by XRD, FTIR, SEM, EDS, BET, and VSM techniques. The FeAl2O4 MNPs act as Lewis acids and offer several advantages such as high yields of products, short reaction times, and easy workup procedure. Moreover, the recycled nanocatalyst was used at least four times without significant loss of its activity.
引用
收藏
页码：5705 / 5723
页数：19
相关论文
共 50 条
  • [1] Synthesis and characterization of spinel FeAl2O4 (hercynite) magnetic nanoparticles and their application in multicomponent reactions
    Arash Ghorbani-Choghamarani
    Masoud Mohammadi
    Lotfi Shiri
    Zahra Taherinia
    Research on Chemical Intermediates, 2019, 45 : 5705 - 5723
  • [2] Kinetics of Hydrogen Reduction of Iron Aluminate FeAl2O4 (Hercynite).
    Gaballah, I.
    Gleitzer, C.
    1600, (73):
  • [3] One-step chemical vapor deposition synthesis of magnetic CNT-hercynite (FeAl2O4) hybrids with good aqueous colloidal stability
    Morales, Noe J.
    Goyanes, Silvia
    Chiliotte, Claudio
    Bekeris, Victoria
    Candal, Roberto J.
    Rubiolo, Gerardo H.
    CARBON, 2013, 61 : 515 - 524
  • [4] CRYSTAL-CHEMISTRY OF SYNTHETIC HERCYNITE (FEAL2O4) FROM XRD STRUCTURAL REFINEMENTS AND MOSSBAUER-SPECTROSCOPY
    LARSSON, L
    ONEILL, HS
    ANNERSTEN, H
    EUROPEAN JOURNAL OF MINERALOGY, 1994, 6 (01) : 39 - 51
  • [5] Synthesis and applications of CoFe2O4 nanoparticles for multicomponent reactions
    Rajput, Jaspreet Kaur
    Kaur, Gagandeep
    CATALYSIS SCIENCE & TECHNOLOGY, 2014, 4 (01) : 142 - 151
  • [6] Structure and magnetic properties of FeAl2O4 synthesized by microwave magnetic field irradiation
    Fukushima, Jun
    Hayashi, Yamato
    Takizawa, Hirotsugu
    JOURNAL OF ASIAN CERAMIC SOCIETIES, 2013, 1 (01): : 41 - 45
  • [7] Crystal structure and Mossbauer study of FeAl2O4
    Jastrzebska, Ilona
    Szczerba, Jacek
    Stoch, Pawel
    Blachowski, Artur
    Ruebenbauer, Krzysztof
    Prorok, Ryszard
    Sniezek, Edyta
    NUKLEONIKA, 2015, 60 (01) : 47 - 49
  • [8] Equation of state of hercynite, FeAl2O4, and high-pressure systematics of Mg-Fe-Cr-Al spinels
    Nestola, F.
    Periotto, B.
    Anzolini, C.
    Andreozzi, G. B.
    Woodland, A. B.
    Lenaz, D.
    Alvaro, M.
    Princivalle, F.
    MINERALOGICAL MAGAZINE, 2015, 79 (02) : 285 - 294
  • [9] Construction and Characterization of Magnetic Fe3O4 Nanoparticles Supported Zn Complex: Research on Multicomponent Synthesis of Highly Functionalized Piperidines
    Xia, Zhao Yan
    Wei, Wu
    Zhang, Li Yan
    CATALYSIS LETTERS, 2024, 154 (07) : 3552 - 3573
  • [10] Magnetic nanocatalysts: Synthesis and application in multicomponent reactions
    Chen, Meng-Nan
    Mo, Li-Ping
    Cui, Zhen-Shui
    Zhang, Zhan-Hui
    CURRENT OPINION IN GREEN AND SUSTAINABLE CHEMISTRY, 2019, 15 : 27 - 37
12345