The crystallization of amorphous Fe2MnGe powder prepared by ball milling

被引：20
|
作者：
Zhang, L [1 ]
Brück, E [1 ]
Tegus, O [1 ]
Buschow, KHJ [1 ]
de Boer, FR [1 ]
机构：
[1] Univ Amsterdam, Van der Waals Zeeman Inst, NL-1018 XE Amsterdam, Netherlands
来源：
JOURNAL OF ALLOYS AND COMPOUNDS | 2003年 / 352卷 / 1-2期
关键词：
transition metal compounds; mechanical alloying; crystal structure; thermal analysis; X-ray diffraction;
D O I：
10.1016/S0925-8388(02)01116-7
中图分类号：
O64 [物理化学（理论化学）、化学物理学];
学科分类号：
070304 ; 081704 ;
摘要：
We synthesized for the first time the intermetallic compound Fe2MnGe. To avoid preferential evaporation of volatile components we exploited mechanical alloying. Amorphous Fe2MnGe alloy powder was prepared by planetary ball milling elemental starting materials. The amorphous-to-crystalline transition was studied by means of differential scanning calorimetry (DSC) and X-ray diffraction (XRD). A cubic D0(3) phase is formed at low temperature and transforms to a high-temperature hexagonal D0(19) phase. The apparent activation energy was determined by means of the Kissinger method. (C) 2002 Elsevier Science B.V. All rights reserved.
引用
收藏
页码：99 / 102
页数：4
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