Tris(1,1,1,3,3,3-hexafluoroisopropyl) phosphate

被引：0

作者：

Saaidi, Pierre-Loic

Jeanneau, Erwann ^{[1
]}

Hasserodt, Jens

机构：

[1] Univ Lyon 1, Ctr Diffractometrie Henri Longchembon, 43 Blvd 11 Novembre 1918, F-69622 Villeurbanne, France

[2] Ecole Normale Super Lyon, Chim Lab, F-69364 Lyon 07, France

来源：

ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS | 2007年 / 63卷

关键词：

D O I：

10.1107/S160053680702853X

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

The title compound, C9H3F18O4P, was synthesized by condensation of sodium hexafluoroisopropanolate and phosphoryl chloride. The P atom is in a distorted tetrahedral environment. The molecules are stabilized by weak O center dot center dot center dot H and F center dot center dot center dot H hydrogen- bond interactions as well as F center dot center dot center dot F interactions.

引用

页码：O3241 / U3779

页数：9

共 18 条

[1] TABLES OF BOND LENGTHS DETERMINED BY X-RAY AND NEUTRON-DIFFRACTION .1. BOND LENGTHS IN ORGANIC-COMPOUNDS [J].

ALLEN, FH ;

KENNARD, O ;

WATSON, DG ;

BRAMMER, L ;

ORPEN, AG ;

TAYLOR, R .

JOURNAL OF THE CHEMICAL SOCIETY-PERKIN TRANSACTIONS 2, 1987, (12) :S1-S19

[2] SIR97:: a new tool for crystal structure determination and refinement [J].

Altomare, A ;

Burla, MC ;

Camalli, M ;

Cascarano, GL ;

Giacovazzo, C ;

Guagliardi, A ;

Moliterni, AGG ;

Polidori, G ;

Spagna, R .

JOURNAL OF APPLIED CRYSTALLOGRAPHY, 1999, 32 :115-119

[3]

[Anonymous], COLLECT

[4] PATTERNS IN HYDROGEN BONDING - FUNCTIONALITY AND GRAPH SET ANALYSIS IN CRYSTALS [J].

BERNSTEIN, J ;

DAVIS, RE ;

SHIMONI, L ;

CHANG, NL .

ANGEWANDTE CHEMIE-INTERNATIONAL EDITION, 1995, 34 (15) :1555-1573

[5] CRYSTALS version 12: software for guided crystal structure analysis [J].

Betteridge, PW ;

Carruthers, JR ;

Cooper, RI ;

Prout, K ;

Watkin, DJ .

JOURNAL OF APPLIED CRYSTALLOGRAPHY, 2003, 36 :1487-1487

[6]

BRANDENBURG KPH, 1996, DIAMOND VERSION 3

[7] PREPARATION AND CHARACTERIZATION OF SOME PHOSPHORUS-COMPOUNDS CONTAINING HEXAFLUOROISOPROPOXY GROUP [J].

DAKTERNIEKS, D ;

ROSCHENTHALER, GV ;

SCHMUTZLER, R .

JOURNAL OF FLUORINE CHEMISTRY, 1978, 11 (3-4) :387-398

[8] Synthesis and comparative analysis of the steric and supramolecular structures of diastereomers of 4,4-bis(trifluoromethyl)-2-(fluoroalkoxy)-6,7-benzo-1,3,2λ5- dioxaphosphepin-5-one 2-oxides [J].

Gubaidullin, AT ;

Mironov, VF ;

Burnaeva, LM ;

Litvinov, IA ;

Dobrynin, AB ;

Goryunov, EI ;

Ivkova, GA ;

Konovalova, IV ;

Mastryukova, TA .

RUSSIAN JOURNAL OF GENERAL CHEMISTRY, 2004, 74 (06) :842-859

[9] Self-assembly of heteroleptic [Cu(dipyrrinato)(hfacac)] complexes directed by fluorine-fluorine interactions [J].

Halper, SR ;

Cohen, SM .

INORGANIC CHEMISTRY, 2005, 44 (12) :4139-4141

[10] Toward a stable hydroxyphosphorane [J].

Hanes, RE ;

Lynch, VM ;

Anslyn, EV ;

Dalby, KN .

ORGANIC LETTERS, 2002, 4 (02) :201-203

← 1 2 →