3-Acetyl-6-chloro-2-methyl-4-phenylquinolinium perchlorate

被引：1

作者：

Shahani, Tara ^{[1
]}

Fun, Hoong-Kun ^{[1
]}

Sarveswari, S. ^{[2
]}

Vijayakumar, V. ^{[2
]}

Reddy, B. Palakshi ^{[2
]}

机构：

[1] Univ Sains Malaysia, Sch Phys, Xray Crystallog Unit, George Town 11800, Malaysia

[2] VIT Univ, Sch Adv Sci, Div Organ Chem, Vellore 632014, Tamil Nadu, India

来源：

ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE | 2010年 / 66卷

关键词：

ONE-POT SYNTHESIS; X-RAY; DIFFRACTION; DERIVATIVES; QUINOLINE;

D O I：

10.1107/S1600536810012900

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

In the title molecular salt, C(18)H(15)ClNO(+)center dot ClO(4)(-), the quinolinium ring system is approximately planar, with a maximum deviation of 0.027 (1) angstrom. The dihedral angle formed between the mean planes of the quinolinium ring system and the benzene ring is 78.46 (3)degrees. In the crystal structure, intermolecular N-H center dot center dot center dot O and C-H center dot center dot center dot O hydrogen bonds link the cations and anions into a three-dimensional network. The crystal structure is further consolidated by C-H center dot center dot center dot pi interactions.

引用

页码：O1192 / U1089

页数：11

共 14 条

[1] TABLES OF BOND LENGTHS DETERMINED BY X-RAY AND NEUTRON-DIFFRACTION .1. BOND LENGTHS IN ORGANIC-COMPOUNDS [J].

ALLEN, FH ;

KENNARD, O ;

WATSON, DG ;

BRAMMER, L ;

ORPEN, AG ;

TAYLOR, R .

JOURNAL OF THE CHEMICAL SOCIETY-PERKIN TRANSACTIONS 2, 1987, (12) :S1-S19

[2]

[Anonymous], 2009, SADABS APEX2 SAINT

[3]

[Anonymous], 1991, SYNLETT

[4] 2,4-DIAMINO-6,7-DIMETHOXYQUINOLINE DERIVATIVES AS ALPHA-1-ADRENOCEPTOR ANTAGONISTS AND ANTIHYPERTENSIVE AGENTS [J].

CAMPBELL, SF ;

HARDSTONE, JD ;

PALMER, MJ .

JOURNAL OF MEDICINAL CHEMISTRY, 1988, 31 (05) :1031-1035

[5] A NITROGEN-GAS-STREAM CRYOSTAT FOR GENERAL X-RAY-DIFFRACTION STUDIES [J].

COSIER, J ;

GLAZER, AM .

JOURNAL OF APPLIED CRYSTALLOGRAPHY, 1986, 19 (02) :105-107

[6] 1-(6-Chloro-2-methyl-4-phenyl-3-quinolyl)ethanone [J].

Fun, Hoong-Kun ;

Loh, Wan-Sin ;

Sarveswari, S. ;

Vijayakumar, V. ;

Reddy, B. Palakshi .

ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2009, 65 :O2688-U244

[7] Zn(II)-mediated alkynylation-cyclization of o-trifluoroacetyl anilines:: One-pot synthesis of 4-trifluoromethyl-substituted quinoline derivatives [J].

Jiang, B ;

Si, YG .

JOURNAL OF ORGANIC CHEMISTRY, 2002, 67 (26) :9449-9451

[8] A convenient and highly regioselective one-pot synthesis of quinolines by addition of a Vilsmeier-type reagent to N-arylimines [J].

Katritzky, AR ;

Arend, M .

JOURNAL OF ORGANIC CHEMISTRY, 1998, 63 (26) :9989-9991

[9] 1-(6-Chloro-2-methyl-4-phenylquinolin-3-yl)-3-(3-methoxyphenyl)prop-2-en-1-one [J].

Loh, Wan-Sin ;

Fun, Hoong-Kun ;

Sarveswari, S. ;

Vijayakumar, V. ;

Reddy, B. Palakshi .

ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2010, 66 :O91-U1821

[10] ANTIPROTOZOAL 4-ARYLOXY-2-AMINOQUINOLINES AND RELATED COMPOUNDS [J].

MARKEES, DG ;

DEWEY, VC ;

KIDDER, GW .

JOURNAL OF MEDICINAL CHEMISTRY, 1970, 13 (02) :324-&

← 1 2 →