A review of oxygen-17 solid-state NMR of organic materials -: towards biological applications

被引：95

作者：

Lemaître, V

Smith, ME

Watts, A

机构：

[1] Univ Oxford, Dept Biochem, Biomembrane Struct Unit, Oxford OX1 3QU, England

[2] Nestec Ltd, BioAnalyt Dept, CH-1000 Lausanne 26, Switzerland

[3] Univ Warwick, Dept Phys, Coventry CV4 7AL, W Midlands, England

来源：

SOLID STATE NUCLEAR MAGNETIC RESONANCE | 2004年 / 26卷 / 3-4期

基金：

英国工程与自然科学研究理事会;

关键词：

oxygen-17; solid-state NMR; MAS; DOR; DAS; MQMAS; amino acids; organic molecules; peptide; hemeprotein; hydrogen-bond; biological applications; review;

D O I：

10.1016/j.ssnmr.2004.04.004

中图分类号：

O64 [物理化学（理论化学）、化学物理学];

学科分类号：

070304 ; 081704 ;

摘要：

O-17 solid state NMR of organic materials is developing rapidly. This article provides a snapshot of the current state of development of this field. The NMR techniques and enrichment protocols that are driving this progress are outlined. The O-17 parameters derived from solid-state NMR experiments are summarized and the structural sensitivity of the approach to effects such as hydrogen bonding highlighted. The prospects and challenges for O-17 solid-state NMR of biomolecules are discussed. (C) 2004 Elsevier Inc. All rights reserved.

引用

页码：215 / 235

页数：21

共 125 条

[1] NEUTRON-DIFFRACTION STUDY OF L-PHENYLALANINE HYDROCHLORIDE [J].