Synthesis and characterization of bismuth titanate by an aqueous sol-gel method

被引：21

作者：

Du, Xianfeng ^{[1
]}

Xu, Youlong ^{[1
]}

Ma, Hanxiao ^{[1
]}

Wang, Jie ^{[1
]}

Li, Xifei ^{[1
]}

机构：

[1] Xi An Jiao Tong Univ, Sch Elect & Informat Engn, Xian 710049, Peoples R China

来源：

JOURNAL OF THE AMERICAN CERAMIC SOCIETY | 2007年 / 90卷 / 05期

关键词：

D O I：

10.1111/j.1551-2916.2007.01548.x

中图分类号：

TQ174 [陶瓷工业]; TB3 [工程材料学];

学科分类号：

0805 ; 080502 ;

摘要：

A highly stable, reproducible and water-based bismuth titanate (BTO) sol system has been synthesized by an aqueous sol-gel method. First bismuth nitrate was dissolved in acetic acid, and then it was mixed with a solution of lactic acid dissolved tetra-n-butyl titanate, subsequently, water was added to adjust sol concentration. As-obtained sols or gels were characterized by Ultraviolet-Visible Spectrophotometer, derivative differential thermal analysis-differential thermal analysis-thermal gravimetry, in situ Raman, and high-temperature X-ray diffraction. Results show that the BTO sol can remain stable for more than 1 year and BTO can start to crystallize at about 450 degrees C.

引用

页码：1382 / 1385

页数：4

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