Analysis of bioactive fluoride-containing calcium aluminosilicate glasses

被引:9
作者
De Maeyer, EAP [1 ]
Verbeeck, RMH [1 ]
机构
[1] State Univ Ghent, Inst Biomed Technol, Sch Dent, Dept Dent Mat Sci, B-9000 Ghent, Belgium
关键词
bioactive fluoride-containing glasses; destructive analysis; decomposition method; AAS; ion-selective electrode;
D O I
10.1016/S0003-2670(97)00591-6
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
Different decomposition methods in aqueous solutions were evaluated on their accuracy and reproducibility for the quantitative determination of the constituents of bioactive fluoride-containing glasses used in dental glass ionomer cements. The concentrations of metals can be determined rapidly and accurately by atomic absorption spectrophotometry after degrading the sample in hydrochloric or hydrofluoric acid. The latter degradation method is also suited for the determination of Si. F can be determined with an ion-selective electrode after degrading the samples in 0.5 M HCl. Higher HCl concentrations enhance the risk of HF release. (C) 1998 Elsevier Science B.V.
引用
收藏
页码:79 / 83
页数:5
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