Silica materials with wall-embedded nitroxides provide efficient polarization matrices for dynamic nuclear polarization NMR

被引：21

作者：

Besson, Eric ^{[1
]}

Ziarelli, Fabio ^{[2
]}

Bloch, Emily ^{[3
]}

Gerbaud, Guillaume ^{[4
]}

Queyroy, Severine ^{[1
]}

Viel, Stephane ^{[1
,5
]}

Gastaldi, Stephane ^{[1
]}

机构：

[1] Aix Marseille Univ, CNRS, ICR UMR 7273, F-13397 Marseille, France

[2] Aix Marseille Univ, Cent Marseille, CNRS, Federat Sci Chim FR 1739, F-13397 Marseille, France

[3] Aix Marseille Univ, CNRS, MADIREL UMR 7246, F-13397 Marseille, France

[4] Aix Marseille Univ, CNRS, BIP UMR 7281, F-13402 Marseille, France

[5] Inst Univ France, F-75005 Paris, France

来源：

CHEMICAL COMMUNICATIONS | 2016年 / 52卷 / 32期

关键词：

SPECTROSCOPY; SOLIDS;

D O I：

10.1039/c6cc01809b

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

Hybrid mesoporous silica materials with wall-embedded nitroxides are shown to efficiently polarize impregnated substrates in high-field dynamic nuclear polarization magic-angle spinning solid-state NMR experiments.

引用

页码：5531 / 5533

页数：3

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