Nickel(II) and cobalt(II) chelates with products of condensation of 1,8-diaminonaphthalene and salycylaldehyde

被引：5
|
作者：
Skorokhod, L. S.
Seifullina, I. I.
Vlasenko, V. G.
Pirog, I. V.
机构：
[1] Mechnikov Univ, UA-270100 Odessa, Ukraine
[2] Rostov State Univ, Phys Res Inst, Rostov Na Donu 344104, Russia
来源：
RUSSIAN JOURNAL OF COORDINATION CHEMISTRY | 2007年 / 33卷 / 05期
关键词：
D O I：
10.1134/S107032840705003X
中图分类号：
O61 [无机化学];
学科分类号：
070301 ; 081704 ;
摘要：
Six Ni(II) and Co(II) chelates were synthesized from different reagents (Ni(II), Co(II) chlorides and 1,8-diaminonaphthalene or the products of a single or double condensation of the latter with salicylaldehyde) and identified and characterized by elemental analysis, powder X-ray diffraction, thermogravimetry, and conductivity methods. The ligand coordination mode and the spatial structure of the complexes were established from the magnetochemisty and spectroscopy (IR, diffuse reflection) data. The dimeric structure of one of the complexes formed due to the chloride bridges was confirmed by EXAFS method.
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收藏
页码：328 / 334
页数：7
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