Fast scanning laser-OES.: I.: Characterization of non-metallic inclusions in steel

被引:21
作者
Kuss, HM
Mittelstädt, H
Müller, G
Nazikkol, C
机构
[1] Gerhard Mercator Univ, D-47057 Duisburg, Germany
[2] ThyssenKrupp Stahl AG, Forsch Zent Qualitats & Prufwesen, Duisburg, Germany
关键词
laser-OES; LIBS; LIPS; low alloy steel; mapping routine; non-metallic inclusion; sample preparation; scanning laser spectrometry; steel cleanness; steel matrix; synthetic sample material;
D O I
10.1081/AL-120018255
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
Pulsed laser sources with high repetition rates, high beam quality and pulse-to-pulse stability are available since few years. These sources can be applied to micro-analytical scanning techniques requiring high number of laser pulses in a short time, low signal deviation and good focusability. A scanning laser-induced optical emission spectrometer (Laser-OES) using such a lasers source was built up and applied to steel cleanness analysis. This novel analytical technique enables to distinguish between different inclusion types based on their chemical compositions. Coincidences of high intensity peaks for single elements at the same co-ordinates can be connected to specific inclusion types.
引用
收藏
页码:659 / 665
页数:7
相关论文
共 19 条
  • [1] BETTE H, 2002, UNPUB P 6 INT WORKSH
  • [2] Bette H., 2001, LASEROPTO, V33, P60
  • [3] BLECK W, 1989, STAHL EISEN, V109, P111
  • [4] CREMERS DA, 2000, ENCY ANAL CHEM, V11
  • [5] *EUR COMM COAL STE, 7210PR168 EUR COMM C
  • [6] Goldstein J.I., 1975, PRACTICAL SCANNING E
  • [7] Jacobi H, 1996, STAHL EISEN, V116, P59
  • [8] Koch W., 1965, METALLKUNDLICHE ANAL
  • [9] MA Z, 2002, CONTROL NONMETALLIC
  • [10] Grain refining of structural steels by dispersion of fine oxide particles
    Ma, ZT
    Peisker, D
    Janke, D
    [J]. STEEL RESEARCH, 1999, 70 (4-5): : 178 - 182