A fiber-optic pipette for rapid long-pathlength capillary spectroscopy

被引:4
|
作者
Stellman, CM [1 ]
Bucholtz, F [1 ]
Ewing, KJ [1 ]
Aggarwal, ID [1 ]
机构
[1] USN, Res Lab, Div Opt Sci, Washington, DC 20375 USA
关键词
fiber-optic pipette; spectroscopy; Raman spectra;
D O I
10.1016/S0925-4005(97)00329-8
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
A fiber-optic pipette (FOP) has been developed. The device uniquely couples a glass capillary, a commun syringe and a single optical fiber to provide for a facile means of achieving long-pathlength capillary spectroscopy. The novel mechanical configuration uf the FOP allows for the acquisition of rapid spectroscopic measurements of small-volume liquid samples while simultaneously achieving signal enhancements of the collected spectroscopic signal. The device has been successful employed in collective the Raman spectra of several solvents, a preliminary characterization of the signal enhancement capabilities has been demonstrated and the advantages associated with the device have been discussed. (C) 1998 Published by Elsevier Science S.A. All rights reserved.
引用
收藏
页码:56 / 60
页数:5
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