N′-[(E)-4-(Diethylamino)benzylidene]-4-nitrobenzohydrazide monohydrate

被引:0
|
作者
Ahmad, Tanveer [2 ]
Zia-ur-Rehman, Muhammad [1 ]
Siddiqui, Hamid Latif [2 ]
Rizvi, Syed Umar Farooq [2 ]
Parvez, Masood [3 ]
机构
[1] Appl Chem Res Ctr, Lahore 54600, Pakistan
[2] Univ Punjab, Inst Chem, Lahore 54590, Pakistan
[3] Univ Calgary, Dept Chem, Calgary, AB T2N 1N4, Canada
来源
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE | 2010年 / 66卷
关键词
COMPLEXES;
D O I
10.1107/S1600536810011554
中图分类号
O7 [晶体学];
学科分类号
0702 ; 070205 ; 0703 ; 080501 ;
摘要
In the title compound, C(18)H(20)N(4)O(3)center dot H(2)O, the two aromatic rings are linked through a methylidenehydrazide fragment, which is fully extended with C-C-N-N, C-N-N=C and N-N=C-C torsion angles of 179.4 (2), 174.7 (2) and 178.3 (2)degrees, respectively. The dihedral angle between the two aromatic rings is 7.01 (8)degrees. In the crystal structure, the water of hydration is involved in extensive hydrogen bonding. Intermolecular O-H center dot center dot center dot O, N-H center dot center dot center dot O and O-H center dot center dot center dot N hydrogen bonds link the components of the structure into a two-dimensional network and additional stabilization is provided by weak intermolecular C-H center dot center dot center dot O hydrogen bonds.
引用
收藏
页码:O1007 / U3791
页数:12
相关论文
共 50 条
  • [31] (E)-N′-[4-(Dimethylamino)benzylidene]-4-hydroxybenzohydrazide hemihydrate
    Liu, Huanyu
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2010, 66 : O1582 - U666
  • [32] (E)-4-Chloro-N-[4-(methylsulfonyl)benzylidene]aniline
    Chen, Yue-Hu
    Wang, Fang
    Li, Guo-Qiang
    Qian, Shao-Song
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2012, 68
  • [33] N'-(2-Hydroxy-5-chlorobenzylidene)-4-nitrobenzohydrazide methanol solvate
    Han, Ling
    Huang, Shan-Shan
    Huang, Qing-Bai
    Zhou, Xue-Mei
    Diao, Yun-Peng
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2008, 64 : O781 - U1220
  • [34] (E)-2-[4-(Diethylamino)styryl]-1-methyl-pyridinium-4-methoxybenzenesulfonate monohydrate
    Chantrapromma, Suchada
    Kaewmanee, Narissara
    Boonnak, Nawong
    Anantapong, Teerasak
    Fun, Hoong-Kun
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2012, 68 : O2728 - +
  • [35] (E)-2-[4-(Diethylamino)styryl]-1-methylpyridinium 4-chlorobenzenesulfonate monohydrate
    Fun, Hoong-Kun
    Kaewmanee, Narissara
    Chanawanno, Kullapa
    Karalai, Chatchanok
    Chantrapromma, Suchada
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2011, 67 : O2488 - U1679
  • [36] New Reactions of Tropylium Salts with 4-Nitrobenzohydrazide, Semicarbazide, Thiosemicarbazide, and N-Benzylurea
    L. P. Yunnikova
    T. A. Akentʼeva
    Yu. E. Likhareva
    Russian Journal of Organic Chemistry, 2020, 56 : 2244 - 2247
  • [37] (E)-2-[4-(Diethylamino)styryl]-1-methylpyridinium benzenesulfonate monohydrate
    Fun, Hoong-Kun
    Kaewmanee, Narissara
    Chanawanno, Kullapa
    Chantrapromma, Suchada
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2011, 67 : O593 - U1493
  • [38] (E)-2-[4-(Diethylamino)styryl]-1-ethylpyridinium iodide monohydrate
    Chantrapromma, Suchada
    Boonnak, Nawong
    Kaewmanee, Narissara
    Quah, Ching Kheng
    Fun, Hoong-Kun
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2013, 69 : O458 - +
  • [39] Crystal growth and characterization of an NLO organic crystal: N′-[(Z)-(4-methylphenyl)methylidene]-4-nitrobenzohydrazide
    Naseema, K.
    Rao, Vijayalakshmi
    Sujith, K. V.
    Kalluraya, Balakrishna
    CURRENT APPLIED PHYSICS, 2010, 10 (04) : 1236 - 1241
  • [40] N′-(3,5-Dichloro-2-hydroxybenzylidene)-4-nitrobenzohydrazide methanol solvate
    Zhu, Hai-Yun
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2010, 66 : O2562 - U468