Synthesis and Crystal Structure of a [70]Fullerene-Pentacene Monoadduct

被引：7

作者：

Shirai, Hitoshi ^{[1
]}

Tajima, Tomoyuki ^{[1
]}

Kubo, Kentaro ^{[1
]}

Nishihama, Takuya ^{[1
]}

Miyake, Hideaki ^{[2
]}

Takaguchi, Yutaka ^{[1
]}

机构：

[1] Okayama Univ, Grad Sch Environm & Life Sci, Kita Ku, 3-1-1 Tsushima Naka, Okayama 7008530, Japan

[2] Yamaguchi Univ, Grad Sch Sci & Engn, 2-16-1 Tokiwadai, Ube, Yamaguchi 7558611, Japan

来源：

BULLETIN OF THE CHEMICAL SOCIETY OF JAPAN | 2016年 / 89卷 / 04期

关键词：

C-60; C-70; FULLERODENDRON; CYCLOADDITION; FABRICATION; FULLERENES; MOLECULES; CHEMISTRY; ADDUCTS;

D O I：

10.1246/bcsj.20150378

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

We succeeded in the first isolation of a single pure regioisomer of a C-70-acene monoadduct. 1,9-Diels-Alder monoadducts of C-70 with pentacene derivatives were obtained by not only the Diels-Alder reaction but also a one-pot reaction using stable dihydropentacene derivatives, 2,3-dichloro-5,6-dicyano-1,4-benzoquinone (DDQ), and C-70. The X-ray crystallographic study of a single pure regioisomer 2b confirmed positions of the linkage between C-70 and acenes for the first time, and revealed unique columnar stacks.

引用

页码：437 / 443

页数：7

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