Synthesis and characterization of twinned flower-like ZnO structures grown by hydrothermal methods

被引:30
|
作者
Sun, Yuanping [1 ]
Guo, Hongying [1 ]
Zhang, Wei [1 ]
Zhou, Taofei [2 ]
Qiu, Yongxin [2 ]
Xu, Ke [2 ]
Zhang, Baoshun [2 ]
Yang, Hui [2 ]
机构
[1] Yantai Univ, Inst Sci & Technol Optoelect Informat, Yantai 264005, Peoples R China
[2] Chinese Acad Sci, Suzhou Inst Nanotech & Nanobion, Suzhou 215123, Peoples R China
基金
中国国家自然科学基金;
关键词
Hydrothermal growth; Semiconducting II-VI materials; ZnO twinned flower-like structure; NANOTUBE ARRAYS; PHOTOLUMINESCENCE; UV;
D O I
10.1016/j.ceramint.2016.03.051
中图分类号
TQ174 [陶瓷工业]; TB3 [工程材料学];
学科分类号
0805 ; 080502 ;
摘要
Twinned flower-like ZnO structures have been synthesized by one-step (TAB assisted hydrothermal methods at a low-temperature as 90 degrees C. Scanning electron microscopy (SEM) and X-ray diffraction (XRD) results disclosed a twinned flower-like morphology and hexagonal wurtzite structures. The XRD pattern and temperature-dependent PL results show a mixed structure of as-grown samples, which are confirmed by the SEM results. The CL spectrum on a single twinned flower-like ZnO structures showed an excellent optical property. Based on experimental results, self-etching and regrowth are suggested as the mechanism to grow the flower-like structures. (C) 2016 Elsevier Ltd and Techna Group S.r.l. All rights reserved.
引用
收藏
页码:9648 / 9652
页数:5
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