The synthesis and properties of high pure δ layered sodium disilicate

被引:4
作者
Dong, J.-X. [1 ]
Li, L.-P.
Xu, H.
Deng, F.
Zhang, G.-Y.
Li, J.-P.
Ai, X.-J.
机构
[1] Taiyuan Univ Technol, Res Inst Special Chem, Taiyuan 030024, Shanxi Province, Peoples R China
[2] Chinese Acad Sci, Wuhan Inst Phys & Math, State Key Lab Magnet Resonance & Atom & Mol Phys, Wuhan 430071, Peoples R China
[3] China Res Inst Daily Chem Ind, Taiyuan 030001, Shanxi Province, Peoples R China
关键词
delta layered sodium disilicate; synthesis; purity;
D O I
10.3139/113.100326
中图分类号
O69 [应用化学];
学科分类号
081704 ;
摘要
delta layered sodium disilicate (delta-Na2Si2O5) is a single layer silicate and has good properties as detergent builder. However, it is difficult to synthesize high pure delta-Na2Si2O5. In this paper, a feasible and simple technology was found by decreasing Na content in liquid sodium silicate (water glass). The crystalline time was short and no seed needed. The suitable synthesis conditions were Si/Na = 1.05 - 1.10, calcining at 720 degrees C for 5 minutes. The synthesis conditions are of industrial value. XRD and Si-29 NIVIR data proved that synthesized samples were delta-Na2Si2O5 without impure phase. High pure delta-Na2Si2O5 exhibited good ions binding ability and reached 312 to 338 mg CaCO3/g.
引用
收藏
页码:34 / 39
页数:6
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