Microwave-enhanced synthesis of thiocarbonohydranzones under solvent-free conditions

被引:0
作者
Bai, YJ [1 ]
Lu, J
Yang, L
Shi, WP
Shi, Z
机构
[1] NW Univ Xian, Dept Chem, Xian 710069, Peoples R China
[2] Xinjiang Talimu Agr Univ, Dept Art & Sci, Alaer 843300, Peoples R China
关键词
solvent-free; microwave irradiation; thiocarbonohydrazide; aromatic aldehyde; thiocarbonohydrazone;
D O I
暂无
中图分类号
O62 [有机化学];
学科分类号
070303 ; 081704 ;
摘要
The microwave-enhanced synthesis of thiocarbonohydrazones, from aromatic aldehydes and thiocarbonohydrazide under solvent-free conditions without catalyst was achieved. This method is a good option to obtain the title compounds in a simple and inexpensive way. Their structures were confirmed by H-1 NMR and IR spectra.
引用
收藏
页码:1472 / 1474
页数:3
相关论文
共 11 条
[1]  
DUVAL C, 1956, MIKROCHIM ACTA, P747
[2]  
GUHA PC, 1925, J INDIAN CHEM SOC, V2, P225
[3]  
JIN QH, 1999, MICROWAVE CHEM
[4]  
KABASHIMA S, 1990, HETEROCYCLES, V31, P1129
[5]  
RAJENDRAN G, 1985, INDIAN J CHEM B, V24, P680
[6]  
RHEE S, 1972, YAKHAK HOEJI, V16, P162
[7]   Some thiazole derivatives. Part I. [J].
Stephen, HW ;
James, FJ .
JOURNAL OF THE CHEMICAL SOCIETY, 1926, :2531-2538
[8]  
Sun X. H., 1999, HUAXUE TONGBAO, V62, P46
[9]  
WILES DM, 1971, Patent No. 2040014
[10]  
Zhang AJ, 2003, CHINESE J ORG CHEM, V23, P281