Growth of bulk single crystal of N-acetyl DL-methionine and its spectral characterization

被引:3
作者
Moovendaran, K. [1 ]
Natarajan, S. [1 ]
机构
[1] Madurai Kamaraj Univ, Sch Phys, Madurai 625021, Tamil Nadu, India
关键词
N-acetyl DL-methionine; MKN setup; IR; UV-vis-NIR; TGA/DTA;
D O I
10.1016/j.saa.2014.07.012
中图分类号
O433 [光谱学];
学科分类号
0703 ; 070302 ;
摘要
Bulk size single crystal of N-acetyl DL-methionine (C7H13NO3S) (1) was grown using a home-made crystal growth setup (MKN setup). The identity of the grown crystal was confirmed by single crystal X-ray diffraction. The modes of vibrations of the functional groups present were assigned using the infrared (IR) spectrum. UV-vis-NIR spectra showed that the crystals have excellent transparency in the visible and infrared regions. The thermal stability and decomposition of the sample was studied by using thermal analysis (TGA/DTA). Photoluminescence excitation studies showed that the emission occurred at 350 nm for the compound. (C) 2014 Elsevier B.V. All rights reserved.
引用
收藏
页码:317 / 320
页数:4
相关论文
共 15 条
[1]  
[Anonymous], 1980, INFRARED CHARACTERIS
[2]   CRYSTAL STRATIFICATION AND SPONTANEOUS SEPARATION OF ENANTIOMERS - CRYSTAL-STRUCTURE OF N-ACETYL-DL-METHIONINEDIETHYLAMIDE [J].
AUBRY, A ;
PROTAS, J ;
CUNG, MT ;
MARRAUD, M .
ACTA CRYSTALLOGRAPHICA SECTION B-STRUCTURAL SCIENCE, 1979, 35 (NOV) :2634-2638
[3]  
AUBRY A, 1971, CR ACAD SCI C CHIM, V273, P959
[4]   Binding of Calcium to Amino Acids (2) The Crystal Structure of N-Acetyl-(DL)-Methionine and Its Calcium Adduct [J].
Kim, Eunice E. ;
Eriks, Klaas .
STRUCTURAL CHEMISTRY, 1990, 1 (2-3) :281-289
[5]   Mercury CSD 2.0 -: new features for the visualization and investigation of crystal structures [J].
Macrae, Clare F. ;
Bruno, Ian J. ;
Chisholm, James A. ;
Edgington, Paul R. ;
McCabe, Patrick ;
Pidcock, Elna ;
Rodriguez-Monge, Lucia ;
Taylor, Robin ;
van de Streek, Jacco ;
Wood, Peter A. .
JOURNAL OF APPLIED CRYSTALLOGRAPHY, 2008, 41 :466-470
[6]  
MATHIESON AM, 1952, ACTA CRYSTALLOGR, V5, P332
[7]   Polymorphism, morphologies and bulk densities of DL-methionine agglomerate crystals [J].
Matsuoka, M ;
Yamanobe, M ;
Tezuka, N ;
Takiyama, H ;
Ishii, H .
JOURNAL OF CRYSTAL GROWTH, 1999, 198 :1299-1306
[8]   Unidirectional growth and characterization of L-tartaric acid single crystals [J].
Moovendaran, K. ;
Natarajan, S. .
JOURNAL OF APPLIED CRYSTALLOGRAPHY, 2013, 46 :993-998
[9]   Simultaneous growth of several materials using a single experimental setup [J].
Moovendaran, K. ;
Sundar, J. Kalyana ;
Natarajan, S. .
JOURNAL OF CRYSTAL GROWTH, 2011, 334 (01) :1-3
[10]  
Moovendaran K., 2013, JCPT, V03, P130, DOI [10.4236/jcpt.2013.34021, DOI 10.4236/JCPT.2013.34021]