X-ray fluorescence determination of manganese in FD&C blue no. 1

被引:0
作者
Hepp, NM [1 ]
机构
[1] US FDA, Off Cosmet & Colors, Washington, DC 20204 USA
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中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
An X-ray fluorescence (XRF) method was developed for determining manganese in FD&C Blue No. 1 from simply prepared pressed pellets. Results were compared with those of atomic absorption spectroscopy (AAS) of acid-digested or ashed samples. Levels of manganese determined by XRF and AAS were equivalent. The limit of detection (3 sigma) for the XRF method was 3 mu g manganese/g dye. The 95% confidence interval at the specification level was 100 + 10 mu g manganese/g dye.
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页码:89 / 92
页数:4
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