Synthesis and Crystal Structure of 2-(Methylsulfony1)-4-(pyridin-3-yl)pyrimidine

被引：0
作者：
Dong, Hua-Ze [1 ]
Zhu, Hai-Bin [2 ]
机构：
[1] Hefei Teachers Coll, Dept Chem & Chem Engn, Hefei 230061, Peoples R China
[2] Southeast Univ, Sch Chem & Chem Engn, Nanjing 211189, Peoples R China
来源：
ASIAN JOURNAL OF CHEMISTRY | 2010年 / 22卷 / 06期
基金：
中国国家自然科学基金;
关键词：
2-(Methylsulfonyl)-4-(pyridin-3-yl)pyrimidine; Hydrogen bonds; Sulfone; COMPLEXES; LIGANDS;
D O I：
暂无
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
A new compound with molecular formula as C(10)H(9)N(3)O(2)S, was derived from 2-(methylthio)-4-(pyridin-3-yl)pyrimidine. The crystal is monoclinic, space group C2/c with unit cell parameters: a = 5.4625 (8) angstrom, b = 10.8235 (16) angstrom, c = 17.520 (3) angstrom, alpha = 90 degrees, beta= 97.460 (3)degrees, gamma = 90 degrees, V = 1027.1 (3) angstrom(3), Z = 4, Mr = 235.00, Dc = 1.521 g/cm(3), mu = 0.300 mm(-1). F(000) = 488. R =0.0443, wR = 0.1061 for 2413 reflections with 1> 2 sigma(1).
引用
收藏
页码：4953 / 4955
页数：3
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