H-bonding schemes of di- and tri-p-benzamides assessed by a combination of electron diffraction, X-ray powder diffraction and solid-state NMR

被引：17

作者：

Gorelik, Tatiana ^{[1
]}

Matveeva, Galina ^{[1
]}

Kolb, Ute ^{[1
]}

Schleuss, Tobias ^{[2
]}

Kilbinger, Andreas F. M. ^{[2
]}

van de Streek, Jacco ^{[3
]}

Bohle, Anne ^{[4
]}

Brunklaus, Gunther ^{[4
]}

机构：

[1] Johannes Gutenberg Univ Mainz, Inst Phys Chem, D-55099 Mainz, Germany

[2] Johannes Gutenberg Univ Mainz, Inst Organ Chem, D-55099 Mainz, Germany

[3] Goethe Univ Frankfurt, Inst Inorgan & Analyt Chem, D-60438 Frankfurt, Germany

[4] Max Planck Inst Polymer Res, D-55128 Mainz, Germany

来源：

CRYSTENGCOMM | 2010年 / 12卷 / 06期

关键词：

HYDROGEN-BONDS; SPIN PAIRS; N-14; NMR; SPECTROSCOPY; RESOLUTION; C-13; TOMOGRAPHY; RANGE;

D O I：

10.1039/b920569a

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

The crystal structures of di- and tri-p-benzamides are solved by a combination of single crystal, electron and powder X-ray diffraction. Different hydrogen-bonding schemes observed in the two structures are described and classified. The hydrogen-bonding networks are correlated to complementary data obtained from multinuclear solid-state NMR.

引用

页码：1824 / 1832

页数：9

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