Synthesis, spectral, and antimicrobial activity of 6-alkylcarbamato-2,10-dichloro-12-trichloromethyl-12H-dibenzo[d,g][1,3,2]-dioxaphosphocin 6-oxides

被引：2

作者：

Kumar, KA ^{[1
]}

Kasthuraiah, M ^{[1
]}

Babu, MFS ^{[1
]}

Reddy, CS ^{[1
]}

机构：

[1] Sri Venkateswara Univ, Dept Chem, Tirupati 517502, Andhra Pradesh, India

来源：

SYNTHETIC COMMUNICATIONS | 2003年 / 33卷 / 05期

关键词：

2,2-bis(2-hydroxy-5-chlorophenyl)-1,1,1-trichloroethane; dichloroisocyanato phosphinyl carbamates/thiocarbamates; dibenzodioxaphosphocin; 6-oxides;

D O I：

10.1081/SCC-120016327

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

6-Alkylcarbamato/alkylthiocarbamato-2,10-dichloro-12-trichloromethyl-12H-dibenzo[d,g][1,3,2]-dioxaphosphocin 6-oxides (4a-f) have been synthesized by the condensation of 2,2-bis-(2-hydroxy-5-chlorophenyl)-1,1,1-trichloroethane (3) with dichlorophosphinyl carbamates (2a-f) of different alcohols/thiols in the presence of triethylamine in dry toluene. The title compounds structures were confirmed by different spectral (elemental, IR and H-1, C-13 & (PNMR)-P-31) studies and found to possess antimicrobial activity.

引用

页码：819 / 825

页数：7

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