One-step synthesis;
Silica nanoparticles;
Hydrophilic and hydrophobic;
Transmission electron microscopy (TEM);
SURFACE;
D O I:
10.1016/j.apt.2016.12.022
中图分类号:
TQ [化学工业];
学科分类号:
0817 ;
摘要:
Hydrophilic and hydrophobic silica nanoparticles were synthesized by a cheap, simple and low temperature one-step method. The method involves a catalytic reaction between ammonium hydroxide, tetraethyl orthosilicate (TEOS) and dichlorodimethylsilane (DDS) in an ethanol solvent. The effects of different parameters such as chemical concentration and reaction temperature were investigated on size of the synthesized silica particles. Characterizations of hydrophilic and hydrophobic particles were performed using dynamic light scattering (DLS), X-ray diffraction analysis (XRD), transmission electron microscopy (TEM), scanning electron microscopy (SEM), fourier transform infrared spectroscopy (FTIR) and thermogravimetric analysis (TGA). According to the results, by reducing the amount of ammonium hydroxide, ethanol and temperature, the size of hydrophilic silica particles can be reduced to 129 +/- 10.4 nm. Other sides, addition of DDS agent caused to silica particles found hydrophobic property and size of the particles reduced to about 65 +/- 6.5 nm. (C) 2016 The Society of Powder Technology Japan. Published by Elsevier B.V. and The Society of Powder Technology Japan. All rights reserved.
机构:
Univ Sains Malaysia, Sch Dent Sci, Kelantan 16150, Kubang Kerian, MalaysiaUniv Sains Malaysia, Sch Dent Sci, Kelantan 16150, Kubang Kerian, Malaysia
Ab Rahman, Ismail
;
Padavettan, Vejayakumaran
论文数: 0引用数: 0
h-index: 0
机构:
Intel Technol Sdn Bhd, Assembly Technol Dev Malaysia, Kedah 09000, Kulim, MalaysiaUniv Sains Malaysia, Sch Dent Sci, Kelantan 16150, Kubang Kerian, Malaysia
机构:
Okayama Univ, Dept Chem Mat, Grad Sch Nat Sci & Technol, Kita Ku, Okayama 7008530, JapanOkayama Univ, Dept Chem Mat, Grad Sch Nat Sci & Technol, Kita Ku, Okayama 7008530, Japan
Gotoh, Kuniaki
;
Kawazu, Takashi
论文数: 0引用数: 0
h-index: 0
机构:
Okayama Univ, Dept Chem Mat, Grad Sch Nat Sci & Technol, Kita Ku, Okayama 7008530, JapanOkayama Univ, Dept Chem Mat, Grad Sch Nat Sci & Technol, Kita Ku, Okayama 7008530, Japan
Kawazu, Takashi
;
Yoshida, Mikio
论文数: 0引用数: 0
h-index: 0
机构:
Okayama Univ, Dept Chem Mat, Grad Sch Nat Sci & Technol, Kita Ku, Okayama 7008530, JapanOkayama Univ, Dept Chem Mat, Grad Sch Nat Sci & Technol, Kita Ku, Okayama 7008530, Japan
Yoshida, Mikio
;
Oshitani, Jun
论文数: 0引用数: 0
h-index: 0
机构:
Okayama Univ, Dept Chem Mat, Grad Sch Nat Sci & Technol, Kita Ku, Okayama 7008530, JapanOkayama Univ, Dept Chem Mat, Grad Sch Nat Sci & Technol, Kita Ku, Okayama 7008530, Japan
机构:
Univ Modena & Reggio Emilia, Dipartimento Ingn Mat & Ambiente, I-41100 Modena, ItalySahand Unit Technol, Nanostruct Mat Res Ctr, Tabriz 513351996, Iran
Marini, Michele
;
Pourabbas, Behzad
论文数: 0引用数: 0
h-index: 0
机构:
Sahand Unit Technol, Nanostruct Mat Res Ctr, Tabriz 513351996, IranSahand Unit Technol, Nanostruct Mat Res Ctr, Tabriz 513351996, Iran
Pourabbas, Behzad
;
Pilati, Francesco
论文数: 0引用数: 0
h-index: 0
机构:
Univ Modena & Reggio Emilia, Dipartimento Ingn Mat & Ambiente, I-41100 Modena, ItalySahand Unit Technol, Nanostruct Mat Res Ctr, Tabriz 513351996, Iran
Pilati, Francesco
;
Fabbri, Paola
论文数: 0引用数: 0
h-index: 0
机构:
Univ Modena & Reggio Emilia, Dipartimento Ingn Mat & Ambiente, I-41100 Modena, ItalySahand Unit Technol, Nanostruct Mat Res Ctr, Tabriz 513351996, Iran
机构:
Univ Sains Malaysia, Sch Dent Sci, Kelantan 16150, Kubang Kerian, MalaysiaUniv Sains Malaysia, Sch Dent Sci, Kelantan 16150, Kubang Kerian, Malaysia
Ab Rahman, Ismail
;
Padavettan, Vejayakumaran
论文数: 0引用数: 0
h-index: 0
机构:
Intel Technol Sdn Bhd, Assembly Technol Dev Malaysia, Kedah 09000, Kulim, MalaysiaUniv Sains Malaysia, Sch Dent Sci, Kelantan 16150, Kubang Kerian, Malaysia
机构:
Okayama Univ, Dept Chem Mat, Grad Sch Nat Sci & Technol, Kita Ku, Okayama 7008530, JapanOkayama Univ, Dept Chem Mat, Grad Sch Nat Sci & Technol, Kita Ku, Okayama 7008530, Japan
Gotoh, Kuniaki
;
Kawazu, Takashi
论文数: 0引用数: 0
h-index: 0
机构:
Okayama Univ, Dept Chem Mat, Grad Sch Nat Sci & Technol, Kita Ku, Okayama 7008530, JapanOkayama Univ, Dept Chem Mat, Grad Sch Nat Sci & Technol, Kita Ku, Okayama 7008530, Japan
Kawazu, Takashi
;
Yoshida, Mikio
论文数: 0引用数: 0
h-index: 0
机构:
Okayama Univ, Dept Chem Mat, Grad Sch Nat Sci & Technol, Kita Ku, Okayama 7008530, JapanOkayama Univ, Dept Chem Mat, Grad Sch Nat Sci & Technol, Kita Ku, Okayama 7008530, Japan
Yoshida, Mikio
;
Oshitani, Jun
论文数: 0引用数: 0
h-index: 0
机构:
Okayama Univ, Dept Chem Mat, Grad Sch Nat Sci & Technol, Kita Ku, Okayama 7008530, JapanOkayama Univ, Dept Chem Mat, Grad Sch Nat Sci & Technol, Kita Ku, Okayama 7008530, Japan
机构:
Univ Modena & Reggio Emilia, Dipartimento Ingn Mat & Ambiente, I-41100 Modena, ItalySahand Unit Technol, Nanostruct Mat Res Ctr, Tabriz 513351996, Iran
Marini, Michele
;
Pourabbas, Behzad
论文数: 0引用数: 0
h-index: 0
机构:
Sahand Unit Technol, Nanostruct Mat Res Ctr, Tabriz 513351996, IranSahand Unit Technol, Nanostruct Mat Res Ctr, Tabriz 513351996, Iran
Pourabbas, Behzad
;
Pilati, Francesco
论文数: 0引用数: 0
h-index: 0
机构:
Univ Modena & Reggio Emilia, Dipartimento Ingn Mat & Ambiente, I-41100 Modena, ItalySahand Unit Technol, Nanostruct Mat Res Ctr, Tabriz 513351996, Iran
Pilati, Francesco
;
Fabbri, Paola
论文数: 0引用数: 0
h-index: 0
机构:
Univ Modena & Reggio Emilia, Dipartimento Ingn Mat & Ambiente, I-41100 Modena, ItalySahand Unit Technol, Nanostruct Mat Res Ctr, Tabriz 513351996, Iran