Simultaneous Determination of Melamine and Clenbuterol in Animal Feeds by GC-MS

被引：48

作者：

Zhao, Li ^{[2
]}

Zhao, Jian ^{[1
]}

Huangfu, Wei-Guo ^{[1
]}

Wu, Yin-Liang ^{[1
]}

机构：

[1] Minist Agr, Supervis Inspect & Testing Ctr Agr Prod Qual & Se, Ningbo 315040, Zhejiang, Peoples R China

[2] Shanghai Agr Tech Extens Serv Ctr, Shanghai 201103, Peoples R China

来源：

CHROMATOGRAPHIA | 2010年 / 72卷 / 3-4期

关键词：

Gas chromatography-mass spectrometry; Animal feedstuffs; Clenbuterol; Melamine; LINKED-IMMUNOSORBENT-ASSAY; TANDEM MASS-SPECTROMETRY; LIQUID-CHROMATOGRAPHY; BETA-AGONISTS; RESIDUES; RACTOPAMINE; VALIDATION; SAMPLES; URINE;

D O I：

10.1365/s10337-010-1643-5

中图分类号：

Q5 [生物化学];

学科分类号：

071010 ; 081704 ;

摘要：

A simple, sensitive and reliable GC-MS method for the simultaneous determination of clenbuterol and melamine in feeds was developed and validated. Samples were extracted with acetonitrile/50 mM HCl solution (1:1 v/v), then the extract was cleaned by extraction with ethyl acetate and solid phase extraction. The samples were derivatized with bis(trimethylsilyl)trifluoroacetamide. The selected ion mode detection method (197, 285, 327, 342 for melamine derivative, 86, 212, 262, 277 for clenbuterol derivative) was used. Recoveries of 70.8-92.0% were obtained. The detection limits were 0.6 A mu g kg(-1) (melamine) and 2.40 A mu g kg(-1) (clenbuterol) in feeds.

引用

页码：365 / 368

页数：4

共 50 条

[41] Determination of Four β2-Agonists in Meat, Liver and Kidney by GC-MS with Dual Internal Standards [J].

Wang, Lian ;

Li, Yuan-Qian ;

Zhou, Yun-Ke ;

Yang, Yuan .

CHROMATOGRAPHIA, 2010, 71 (7-8) :737-739

[42] GC-MS and GC-MS/MS measurement of the cardiovascular risk factor homoarginine in biological samples [J].

Kayacelebi, Arslan Arinc ;

Beckmann, Bibiana ;

Gutzki, Frank-Mathias ;

Jordan, Jens ;

Tsikas, Dimitrios .

AMINO ACIDS, 2014, 46 (09) :2205-2217

[43] Optimized conditions for simultaneous determination of opiates, cocaine and benzoylecgonine in hair samples by GC-MS [J].

Romolo, FS ;

Rotolo, MC ;

Palmi, I ;

Pacifici, R ;

Lopez, A .

FORENSIC SCIENCE INTERNATIONAL, 2003, 138 (1-3) :17-26

[44] Simultaneous Determination of Four Alkaloids in Gan-Yan-Ling Injection by GC-MS [J].

Chen, Na ;

Han, Zheng ;

Luan, Lianjun ;

Wu, Yongjiang .

CHROMATOGRAPHIA, 2009, 70 (1-2) :299-303

[45] GC-MS Method for Simultaneous Determination of Four Sedative Hypnotic Residues in Swine Tissues [J].

Cheng, Linli ;

Zhang, Yujie ;

Shen, Jianzhong ;

Wu, Congming ;

Zhang, Suxia .

CHROMATOGRAPHIA, 2010, 71 (1-2) :155-158

[46] Simultaneous Determination of Four Alkaloids in Gan-Yan-Ling Injection by GC-MS [J].

Na Chen ;

Zheng Han ;

Lianjun Luan ;

Yongjiang Wu .

Chromatographia, 2009, 70 :299-303

[47] Preparation of Monoclonal Antibody for Melamine and Development of an Indirect Competitive ELISA for Melamine Detection in Raw Milk, Milk Powder, and Animal Feeds [J].

Yin, Weiwei ;

Liu, Jinting ;

Zhang, Taichang ;

Li, Weihua ;

Liu, Wei ;

Meng, Meng ;

He, Fangyang ;

Wan, Yuping ;

Feng, Caiwei ;

Wang, Shanliang ;

Lu, Xiao ;

Xi, Rimo .

JOURNAL OF AGRICULTURAL AND FOOD CHEMISTRY, 2010, 58 (14) :8152-8157

[48] NSAIDs Determination in Human Serum by GC-MS [J].

Krokos, Adamantios ;

Tsakelidou, Elisavet ;

Michopoulou, Eleni ;

Raikos, Nikolaos ;

Theodoridis, Georgios ;

Gika, Helen .

SEPARATIONS, 2018, 5 (03)

[49] Determination of Tyramine in Hair Samples by GC-MS [J].

Gao, Lina ;

Yuan, Huiya ;

Zhu, Juan ;

Hara, Kenji ;

Liu, Junting .

CHROMATOGRAPHIA, 2016, 79 (1-2) :103-108

[50] Determination of Aniline in Soil by ASE/GC-MS [J].

Shi, Yongli ;

Zhang, Kai .

MOLECULES, 2022, 27 (07)

← 1 2 3 4 5 →